(CH₃)3SnC(CH₂C₆H₅)CHSn(CH₃)3

Base Information

Chemical Name:(CH₃)3SnC(CH₂C₆H₅)CHSn(CH₃)3
CAS No.:85263-65-6
Molecular Formula:C₁₅H₂₆Sn₂
Molecular Weight:443.791
Hs Code.:

(CH<sub>3</sub>)3SnC(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)CHSn(CH<sub>3</sub>)3

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Chemical Property of (CH₃)3SnC(CH₂C₆H₅)CHSn(CH₃)3

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Technology Process of (CH₃)3SnC(CH₂C₆H₅)CHSn(CH₃)3

There total 2 articles about (CH₃)3SnC(CH₂C₆H₅)CHSn(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 10147-11-2
propargyl benzene

: 661-69-8
hexamethyldistannane

: 85263-65-6
(CH₃)3SnC(CH₂C₆H₅)CHSn(CH₃)3

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In neat (no solvent); heating under inert gas, 85°C, 63 h; distn.;
DOI:10.1016/S0022-328X(00)99691-8

Reference yield:

: 87673-32-3
1-trimethylstannyl-3-phenylpropyne

: 1631-73-8
trimethylstannane

: 85263-65-6
(CH₃)3SnC(CH₂C₆H₅)CHSn(CH₃)3

: 87673-36-7
C₆H₅CH₂CHC(Sn(CH₃)3)2

Guidance literature:: With catalyst: azobisisobutyronitrile; In neat (no solvent); equimolar amts. of the alkyne and Me3SnH were heated at 70°C under Ar in the presence of a catalytic amt. of AIBN for 3-4 h (IR and (1)H NMR monitoring); PhCH2CH=C(SnMe3)2 to PhCH2(Me3Sn)C=CHSnMe3 ratio 91:9, total yield 94%; the reaction mixt. was distilled under reduced pressure (b.p. 95°C/0.001 mm Hg); elem. anal. for the isomeric mixt., isomers were not sepd.;
DOI:10.1016/0022-328X(83)80057-6