Technology Process of C17H24O4
There total 5 articles about C17H24O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / tetrahydrofuran; methanol / 1 h / Reflux
2.1: lithium borohydride / tetrahydrofuran; methanol; diethyl ether / 1 h / 0 °C
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C
3.2: -78 - 0 °C
4.1: potassium tert-butylate / tetrahydrofuran; toluene / 1.5 h / 20 °C
4.2: 20 °C
With
lithium borohydride; oxalyl dichloride; potassium tert-butylate; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; dimethyl sulfoxide;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
4.1: Wittig reaction / 4.2: Wittig reaction;
DOI:10.1055/s-0030-1260586
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C
1.2: -78 - -45 °C
2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / Inert atmosphere; Reflux
3.1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / tetrahydrofuran; methanol / 1 h / Reflux
4.1: lithium borohydride / tetrahydrofuran; methanol; diethyl ether / 1 h / 0 °C
5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C
5.2: -78 - 0 °C
6.1: potassium tert-butylate / tetrahydrofuran; toluene / 1.5 h / 20 °C
6.2: 20 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium borohydride; oxalyl dichloride; potassium tert-butylate; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; dimethyl sulfoxide;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
6.1: Wittig reaction / 6.2: Wittig reaction;
DOI:10.1055/s-0030-1260586
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium borohydride / tetrahydrofuran; methanol; diethyl ether / 1 h / 0 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C
2.2: -78 - 0 °C
3.1: potassium tert-butylate / tetrahydrofuran; toluene / 1.5 h / 20 °C
3.2: 20 °C
With
lithium borohydride; oxalyl dichloride; potassium tert-butylate; dimethyl sulfoxide;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
3.1: Wittig reaction / 3.2: Wittig reaction;
DOI:10.1055/s-0030-1260586