2-({1-[2-(2-{[3-(2,4-Dinitro-phenoxy)-pyridine-2-carbonyl]-amino}-3-{2-[(4-oxo-piperidine-2-carbonyl)-amino]-2-phenyl-acetoxy}-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid; compound with trifluoro-acetic acid

Base Information

• Chemical Name: 2-({1-[2-(2-{[3-(2,4-Dinitro-phenoxy)-pyridine-2-carbonyl]-amino}-3-{2-[(4-oxo-piperidine-2-carbonyl)-amino]-2-phenyl-acetoxy}-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid; compound with trifluoro-acetic acid
• CAS No.: 127092-17-5
• Molecular Formula: C₂HF₃O₂*C₄₉H₅₃N₉O₁₅
• Molecular Weight: 1122.04

Synonyms:

Chemical Property of 2-({1-[2-(2-{[3-(2,4-Dinitro-phenoxy)-pyridine-2-carbonyl]-amino}-3-{2-[(4-oxo-piperidine-2-carbonyl)-amino]-2-phenyl-acetoxy}-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid; compound with trifluoro-acetic acid

Chemical Property:

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Technology Process of 2-({1-[2-(2-{[3-(2,4-Dinitro-phenoxy)-pyridine-2-carbonyl]-amino}-3-{2-[(4-oxo-piperidine-2-carbonyl)-amino]-2-phenyl-acetoxy}-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid; compound with trifluoro-acetic acid

There total 3 articles about 2-({1-[2-(2-{[3-(2,4-Dinitro-phenoxy)-pyridine-2-carbonyl]-amino}-3-{2-[(4-oxo-piperidine-2-carbonyl)-amino]-2-phenyl-acetoxy}-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-(2,4-Dinitro-phenoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-yl)-amide (127092-11-9) + trifluoroacetic acid (76-05-1) → 2-({1-[2-(2-{[3-(2,4-Dinitro-phenoxy)-pyridine-2-carbonyl]-amino}-3-{2-[(4-oxo-piperidine-2-carbonyl)-amino]-2-phenyl-acetoxy}-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid; compound with trifluoro-acetic acid (127092-17-5)

Guidance literature:

for 65h; Ambient temperature;

Reference yield:

virginiamycin S1 (668-72-4,23152-29-6,117603-96-0) → 2-({1-[2-(2-{[3-(2,4-Dinitro-phenoxy)-pyridine-2-carbonyl]-amino}-3-{2-[(4-oxo-piperidine-2-carbonyl)-amino]-2-phenyl-acetoxy}-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid; compound with trifluoro-acetic acid (127092-17-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 535 mg / 1,8-bis(dimethylamino)naphthalene / dimethylformamide / 64 h

2: 80 percent / 65 h / Ambient temperature

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In N,N-dimethyl-formamide;

Reference yield:

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → 2-({1-[2-(2-{[3-(2,4-Dinitro-phenoxy)-pyridine-2-carbonyl]-amino}-3-{2-[(4-oxo-piperidine-2-carbonyl)-amino]-2-phenyl-acetoxy}-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid; compound with trifluoro-acetic acid (127092-17-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 535 mg / 1,8-bis(dimethylamino)naphthalene / dimethylformamide / 64 h

2: 80 percent / 65 h / Ambient temperature

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In N,N-dimethyl-formamide;

upstream raw materials:

3-(2,4-Dinitro-phenoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-yl)-amide

trifluoroacetic acid

virginiamycin S₁

2,4-Dinitrofluorobenzene

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