1-ureido-2-carbamoyl-3,6-dimethoxybenzene

Base Information

Chemical Name:1-ureido-2-carbamoyl-3,6-dimethoxybenzene
CAS No.:98991-69-6
Molecular Formula:C₁₀H₁₃N₃O₄
Molecular Weight:239.231
Hs Code.:

Synonyms:

Suppliers and Price of 1-ureido-2-carbamoyl-3,6-dimethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-ureido-2-carbamoyl-3,6-dimethoxybenzene

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Technology Process of 1-ureido-2-carbamoyl-3,6-dimethoxybenzene

There total 1 articles about 1-ureido-2-carbamoyl-3,6-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26002-58-4
2,5-dimethoxy-6-nitrobenzamide

: 98991-69-6
1-ureido-2-carbamoyl-3,6-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / H₂ / 5percent Pd/C / aq. ethanol / 4 h / 2585.7 Torr

2: glacial acetic acid / H₂O / 12 h / Ambient temperature

With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; water;
DOI:10.1021/jo00224a042

Reference yield:

: 98991-69-6
1-ureido-2-carbamoyl-3,6-dimethoxybenzene

: 8-(phenylimino)-6-acetamidoquinazoline-2,4,5-(1H,3H)-trione

Guidance literature:: Multi-step reaction with 6 steps

1: 48 percent / NaOH / H₂O / 2 h / Heating

2: 100 percent / conc. HNO₃, conc. H₂SO₄ / acetic acid

3: H₂, aq. KOH / 5percent Pd/C / 0.5 h / 2585.7 Torr

4: acetic acid / 2 h / Ambient temperature

5: 76 percent / fuming HNO₃ / 0.5 h

6: 20 percent / dimethylformamide / 0.03 h / Heating

With potassium hydroxide; sodium hydroxide; sulfuric acid; hydrogen; nitric acid; acetic acid; palladium on activated charcoal; In water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jo00224a042