3,6-Dimethoxy-2-nitrobenzamide

Base Information

Chemical Name:3,6-Dimethoxy-2-nitrobenzamide
CAS No.:26002-58-4
Molecular Formula:C9H10N2O5
Molecular Weight:226.18600
Hs Code.:
DSSTox Substance ID:DTXSID60358478
Wikidata:Q82139079
ChEMBL ID:CHEMBL1300732
Mol file:26002-58-4.mol

Synonyms:3,6-dimethoxy-2-nitrobenzamide;2-nitro-3,6-dimethoxybenzamide;26002-58-4;Benzamide, 3,6-dimethoxy-2-nitro-;MLS000702389;SMR000226373;Oprea1_128452;cid_899770;CHEMBL1300732;BDBM82772;3,6-dimethoxy-2-nitro-benzamide;DTXSID60358478;HMS2740O23;AG-777/36176052

Suppliers and Price of 3,6-Dimethoxy-2-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 3,6-Dimethoxy-2-nitrobenzamide

Chemical Property:

PSA：108.36000
LogP:2.11830
XLogP3:-0.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:226.05897142
Heavy Atom Count:16
Complexity:278

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)OC)[N+](=O)[O-])C(=O)N

Technology Process of 3,6-Dimethoxy-2-nitrobenzamide

There total 4 articles about 3,6-Dimethoxy-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.8%

: 42020-21-3
2,5-dimethoxybenzamide

: 26002-58-4
2,5-dimethoxy-6-nitrobenzamide

Guidance literature:: With nitric acid; at 15 ℃; for 0.833333h;
DOI:10.1016/S0040-4020(01)89723-4

Reference yield:

: 490-79-9
2,5-dihydroxybenzoic acid.

: 26002-58-4
2,5-dimethoxy-6-nitrobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: aq. KOH / ethanol

2: H₂SO₄

3: aq. NH₃

4: HNO₃

With potassium hydroxide; ammonium hydroxide; sulfuric acid; nitric acid; In ethanol;
DOI:10.1039/j39700000583

Reference yield:

: 2150-40-5
methyl 2,5-dimethoxybenzoate

: 26002-58-4
2,5-dimethoxy-6-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / conc. NH₄OH / Ambient temperature

2: 91.8 percent / 70percent HNO₃ / 0.83 h / 15 °C

With ammonium hydroxide; nitric acid;
DOI:10.1016/S0040-4020(01)89723-4