propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside
CAS No.:129163-04-8
Molecular Formula:C₅₅H₅₉NO₁₅
Molecular Weight:974.071
Hs Code.:

propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Synonyms:

Suppliers and Price of propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Useful:

Technology Process of propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

There total 4 articles about propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110426-17-0
Acetic acid (2R,3S,4S,5R,6R)-5-acetoxy-4-allyloxy-2-allyloxymethyl-6-chloro-tetrahydro-pyran-3-yl ester

: 129163-04-8
propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / AgOSO₃CF₃, 4A molecular sieves / 1,2-dichloro-ethane / 18 h / -10 - 20 °C

2: 91 percent / 1.25 M LiOH, 31percent aq. H₂O₂ / tetrahydrofuran / 13 h / 0 °C

3: 90 percent / Ag₂O, KI / dimethylformamide / 5 h / 0 - 20 °C

With lithium hydroxide; silver trifluoromethane sulfate; 4 A molecular sieve; dihydrogen peroxide; potassium iodide; silver(l) oxide; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84224-I

Reference yield:

: 125946-67-0
allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

: 129163-04-8
propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / AgOSO₃CF₃, 4A molecular sieves / 1,2-dichloro-ethane / 18 h / -10 - 20 °C

2: 91 percent / 1.25 M LiOH, 31percent aq. H₂O₂ / tetrahydrofuran / 13 h / 0 °C

3: 90 percent / Ag₂O, KI / dimethylformamide / 5 h / 0 - 20 °C

With lithium hydroxide; silver trifluoromethane sulfate; 4 A molecular sieve; dihydrogen peroxide; potassium iodide; silver(l) oxide; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84224-I

Reference yield:

: 129163-00-4
allyl O-(3,6-di-O-allyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

: 129163-04-8
propyl O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / Ag₂O, KI / dimethylformamide / 5 h / 0 - 20 °C

With potassium iodide; silver(l) oxide; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84224-I