10,11-Dihydroxy-8,9,10,11-tetrahydroanthracene

Base Information

• Chemical Name: 10,11-Dihydroxy-8,9,10,11-tetrahydro
• Molecular Formula: C₁₈H₁₆O₂
• Molecular Weight: 264.324

Synonyms:

Chemical Property of 10,11-Dihydroxy-8,9,10,11-tetrahydro

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

There total 2 articles about 10,11-Dihydroxy-8,9,10,11-tetrahydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(10R,11S)-10,11-Dihydro-benzo[a]anthracene-10,11-diol (58409-57-7,60839-19-2,60967-90-0,67262-33-3,72522-88-4,72522-89-5,91423-03-9) → (10R,11S)-8,9,10,11-Tetrahydro-benzo[a]anthracene-10,11-diol (79252-28-1,91384-62-2,94903-89-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; Ambient temperature;

DOI:10.1016/S0040-4039(00)91907-5

Reference yield:

8,9-Dihydrobenzanthracene (60968-17-4) → 10,11-Dihydroxy-8,9,10,11-tetrahydroanthracene (79252-28-1,91384-62-2,94903-89-6)

Guidance literature:

With osmium(VIII) oxide; 1) pyridine, 30 min, 0 deg -> ambient temperature, 2) aq. sodium bisulfite, methanol, 48 h;

DOI:10.1021/jo00193a033

Reference yield: 43.0%

(-)-methoxytrifluoromethylphenylacetyl chloride (39637-99-5) + 10,11-Dihydroxy-8,9,10,11-tetrahydroanthracene (79252-28-1,91384-62-2,94903-89-6) → 3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10R,11S)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester (91422-89-8) + 3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester (91365-99-0)

Guidance literature:

In pyridine; 1) 0 deg C, 2 h, 2) ambient temperature, 10 h;

DOI:10.1021/jo00193a033

upstream raw materials:

8,9-Dihydrobenzanthracene

(10R,11S)-10,11-Dihydro-benzo[a]anthracene-10,11-diol

Downstream raw materials:

3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10R,11S)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester

3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester

(+)-cis-(10S,11R)-10,11-Dihydroxy-8,9,10,11-tetrahydrobenzanthracene

C₃₂H₂₄O₄

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