Technology Process of 5,8-dioxa-16-benzoyl-2-hydroxy-1,6(1,3),3(1,4)-tribenzenacyclooctaphane
There total 6 articles about 5,8-dioxa-16-benzoyl-2-hydroxy-1,6(1,3),3(1,4)-tribenzenacyclooctaphane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water; dichloromethane / 12 h / 0 - 20 °C
2: sodium tetrahydroborate / methanol / 5 h / 0 - 20 °C
3: hydrogen bromide / acetic acid / 3 h / 20 °C
4: potassium carbonate / acetone / 24 h
5: potassium hydroxide / methanol / 3 h / 65 °C
6: potassium carbonate / acetone / 79 h / 60 °C
7: benzene / Inert atmosphere; Irradiation
With
sodium tetrahydroborate; N-benzyl-N,N,N-triethylammonium chloride; hydrogen bromide; potassium carbonate; potassium hydroxide; sodium hydroxide;
In
methanol; dichloromethane; water; acetic acid; acetone; benzene;
DOI:10.1039/c2pp25025j
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium tetrahydroborate / methanol / 5 h / 0 - 20 °C
2: hydrogen bromide / acetic acid / 3 h / 20 °C
3: potassium carbonate / acetone / 24 h
4: potassium hydroxide / methanol / 3 h / 65 °C
5: potassium carbonate / acetone / 79 h / 60 °C
6: benzene / Inert atmosphere; Irradiation
With
sodium tetrahydroborate; hydrogen bromide; potassium carbonate; potassium hydroxide;
In
methanol; acetic acid; acetone; benzene;
DOI:10.1039/c2pp25025j
