C₂₈H₂₅N₇O₄S

Base Information

Chemical Name:C₂₈H₂₅N₇O₄S
CAS No.:1466564-89-5
Molecular Formula:C₂₈H₂₅N₇O₄S
Molecular Weight:555.617
Hs Code.:

C<sub>28</sub>H<sub>25</sub>N<sub>7</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₂₈H₂₅N₇O₄S

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Technology Process of C₂₈H₂₅N₇O₄S

There total 7 articles about C₂₈H₂₅N₇O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21327-86-6
2-chloro-6-methylbenzoic acid

: 1466564-89-5
C₂₈H₂₅N₇O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 2 h / 20 °C

1.2: 2 h / 25 - 40 °C / Cooling with ice

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere

2.2: 2 h / -30 - -10 °C / Inert atmosphere

2.3: 10.5 h / 20 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5.1: XPhos; dichloro bis(acetonitrile) palladium(II); propiononitrile; caesium carbonate / dimethyl sulfoxide / 2 h / 103 °C / Sealed tube

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C

With dichloro bis(acetonitrile) palladium(II); n-butyllithium; oxalyl dichloride; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; propiononitrile; XPhos; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 1386861-46-6
2-chloro-6-methyl-N-phenylbenzamide

: 1466564-89-5
C₂₈H₂₅N₇O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere

1.2: 2 h / -30 - -10 °C / Inert atmosphere

1.3: 10.5 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4.1: XPhos; dichloro bis(acetonitrile) palladium(II); propiononitrile; caesium carbonate / dimethyl sulfoxide / 2 h / 103 °C / Sealed tube

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C

With dichloro bis(acetonitrile) palladium(II); n-butyllithium; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; propiononitrile; XPhos; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 89894-44-0
2-chloro-6-methylbenzoyl chloride

: 1466564-89-5
C₂₈H₂₅N₇O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 0.17 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere

2.2: 2 h / -30 - -10 °C / Inert atmosphere

2.3: 10.5 h / 20 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5.1: XPhos; dichloro bis(acetonitrile) palladium(II); propiononitrile; caesium carbonate / dimethyl sulfoxide / 2 h / 103 °C / Sealed tube

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C

With dichloro bis(acetonitrile) palladium(II); n-butyllithium; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; propiononitrile; XPhos; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;