C₁₅H₂₁N₂O⁽¹⁺⁾*Br^(1-)

Base Information

• Chemical Name: C₁₅H₂₁N₂O⁽¹⁺⁾*Br^(1-)
• CAS No.: 1589595-92-5
• Molecular Formula: Br*C₁₅H₂₁N₂O
• Molecular Weight: 325.249
• Mol file: 1589595-92-5.mol

Synonyms:

Chemical Property of C₁₅H₂₁N₂O⁽¹⁺⁾*Br^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₅H₂₁N₂O⁽¹⁺⁾*Br^(1-)

There total 1 articles about C₁₅H₂₁N₂O⁽¹⁺⁾*Br^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

1-benzyl-2-isopropylimidazole (18994-85-9) + 2-bromoethanol (540-51-2) → C15H21N2O(1+)*Br(1-) (1589595-92-5)

Guidance literature:

In acetonitrile; at 80 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1039/c3gc42346h

Reference yield:

C15H21N2O(1+)*Br(1-) (1589595-92-5) → C15H20N2O

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 2h; Schlenk technique; Inert atmosphere;

DOI:10.1039/c3gc42346h

Reference yield:

C15H21N2O(1+)*Br(1-) (1589595-92-5) → C16H20N2O3 (1589596-00-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Schlenk technique; Inert atmosphere

2: tetrahydrofuran / 2 h / -78 - 20 °C / 760.05 Torr / Schlenk technique; Inert atmosphere

With potassium tert-butylate; In tetrahydrofuran;

DOI:10.1039/c3gc42346h

upstream raw materials:

1-benzyl-2-isopropylimidazole

2-bromoethanol

Downstream raw materials:

C₁₆H₂₀N₂O₃

C₁₅H₂₁N₂O⁽¹⁺⁾*CHO₃^(1-)