ethyl (methylsulfanyl)phenylsulfonylacetate

Base Information

• Chemical Name: ethyl (methylsulfanyl)phenylsulfonylacetate
• CAS No.: 190672-15-2
• Molecular Formula: C₁₁H₁₄O₄S₂
• Molecular Weight: 274.362
• Mol file: 190672-15-2.mol

Synonyms:

Chemical Property of ethyl (methylsulfanyl)phenylsulfonylacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl (methylsulfanyl)phenylsulfonylacetate

There total 3 articles about ethyl (methylsulfanyl)phenylsulfonylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium benzenesulfonate (873-55-2) → ethyl (methylsulfanyl)phenylsulfonylacetate (190672-15-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / ethanol / 12 h / Heating

2: 1.) K₂CO₃, triethylbenzylammonium chloride / 1.) benzene, RT, 1 h, 2.) benzene, RT, 1 h

With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In ethanol;

DOI:10.1055/s-1997-1212

Reference yield:

methanethiosulfonic acid S-methyl ester (2949-92-0,31761-75-8) + ethyl 2-phenylsulfonylacetate (7605-30-3) → ethyl (methylsulfanyl)phenylsulfonylacetate (190672-15-2)

Guidance literature:

With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; Yield given. Multistep reaction; 1.) benzene, RT, 1 h, 2.) benzene, RT, 1 h;

DOI:10.1055/s-1997-1212

Reference yield:

S-methyl benzenethiosulfonate (1125-25-3) + ethyl 2-phenylsulfonylacetate (7605-30-3) → ethyl (methylsulfanyl)phenylsulfonylacetate (190672-15-2)

Guidance literature:

With ethanol; sodium carbonate;

DOI:10.1039/jr9320001819

upstream raw materials:

S-methyl benzenethiosulfonate

ethyl 2-phenylsulfonylacetate

methanethiosulfonic acid S-methyl ester

sodium benzenesulfonate

Downstream raw materials:

1-benzenesulfonyl-1-methanesulfonyl-ethane

benzenesulfonyl-bis-methanesulfonyl-methane

methylsulphonyl(phenylsulphonyl)methane

(methylsulfanyl)methyl phenyl sulfone

Refernces