2-diphenylphosphanyl-4-methylphenyl trimethylstannyl ether

Base Information

Chemical Name:2-diphenylphosphanyl-4-methylphenyl trimethylstannyl ether
CAS No.:185509-39-1
Molecular Formula:C₂₂H₂₅OPSn
Molecular Weight:455.124
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Chemical Property of 2-diphenylphosphanyl-4-methylphenyl trimethylstannyl ether

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Technology Process of 2-diphenylphosphanyl-4-methylphenyl trimethylstannyl ether

There total 1 articles about 2-diphenylphosphanyl-4-methylphenyl trimethylstannyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 6627-55-0
2-bromo-p-cresol

: 1066-45-1
trimethyltin(IV)chloride

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 185509-39-1
2-diphenylphosphanyl-4-methylphenyl trimethylstannyl ether

: 185509-41-5
n-butyldiphenyl-((5-methyl-2-trimethylstannyloxy)phenyl)phosphonium bromide

Guidance literature:: With n-BuLi; In diethyl ether; hexane; pentane; (argon); addn. of n-BuLi in hexane to the bromophenol in Et2O, addn. of ClPPh2 in pentane at -30°C, stirring (3 h), addn. of Me3SnCl in pentane, stirring (6 h); filtration, washing (Et2O), evapn., dissoln. (Et2O), pptn. with hexane, drying (vac.), the byproduct being isolated from the crude filtrate after 2 months;
DOI:10.1002/cber.19961291223