C₃₁H₄₁NO₇

Base Information

Chemical Name:C₃₁H₄₁NO₇
CAS No.:88820-83-1
Molecular Formula:C₃₁H₄₁NO₇
Molecular Weight:539.669
Hs Code.:

C<sub>31</sub>H<sub>41</sub>NO<sub>7</sub>

Synonyms:

Suppliers and Price of C₃₁H₄₁NO₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₄₁NO₇

Chemical Property:

Purity/Quality:

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Technology Process of C₃₁H₄₁NO₇

There total 10 articles about C₃₁H₄₁NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33159-45-4
1,2/3,4-bis(O-cyclohexylidene)-α-D-galactopyranose

: 88820-83-1
C₃₁H₄₁NO₇

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) oxalyl chloride, DMSO; 2.) triethylamine / 1.) CH₂Cl₂, -10 deg C, 15 min; 2.) -60 deg C -> room temp.

2: 95 percent / p-toluenesulfonic acid, molecular sieves 4A / benzene / 3 h / Heating

3: 1.) butyllithium, diisopropylamine, HMPT / 1.) THF, hexane, -78 deg C, 30 min; 2.) -70 deg C, 2 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; oxalyl dichloride; 4 A molecular sieve; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; diisopropylamine; In benzene;
DOI:10.1055/s-1983-30512

Reference yield:

: 33159-45-4
1,2/3,4-bis(O-cyclohexylidene)-α-D-galactopyranose

: 88820-83-1
C₃₁H₄₁NO₇

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) oxalyl chloride, DMSO; 2.) triethylamine / 1.) CH₂Cl₂, -10 deg C, 15 min; 2.) -60 deg C -> room temp.

2: 95 percent / p-toluenesulfonic acid, molecular sieves 4A / benzene / 3 h / Heating

3: 1.) butyllithium, diisopropylamine, HMPT / 1.) THF, hexane, -78 deg C, 30 min; 2.) -70 deg C, 2 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; oxalyl dichloride; 4 A molecular sieve; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; diisopropylamine; In benzene;
DOI:10.1055/s-1983-30512

Reference yield:

: 59-23-4
D-Galactose

: 88820-83-1
C₃₁H₄₁NO₇

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / conc. H₂SO₄ / dioxane / 2 h / Ambient temperature

2: 1.) oxalyl chloride, DMSO; 2.) triethylamine / 1.) CH₂Cl₂, -10 deg C, 15 min; 2.) -60 deg C -> room temp.

3: 95 percent / p-toluenesulfonic acid, molecular sieves 4A / benzene / 3 h / Heating

4: 1.) butyllithium, diisopropylamine, HMPT / 1.) THF, hexane, -78 deg C, 30 min; 2.) -70 deg C, 2 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; oxalyl dichloride; 4 A molecular sieve; sulfuric acid; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; diisopropylamine; In 1,4-dioxane; benzene;
DOI:10.1055/s-1983-30512