1-{3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionyl}-pyrrolidine-2-carboxylic acid; hydriodide

Base Information

Chemical Name:1-{3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionyl}-pyrrolidine-2-carboxylic acid; hydriodide
CAS No.:118964-78-6
Molecular Formula:C₂₈H₃₀N₄O₆S₂*HI
Molecular Weight:710.614
Hs Code.:

1-{3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionyl}-pyrrolidine-2-carboxylic acid; hydriodide

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Chemical Property of 1-{3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionyl}-pyrrolidine-2-carboxylic acid; hydriodide

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Technology Process of 1-{3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionyl}-pyrrolidine-2-carboxylic acid; hydriodide

There total 8 articles about 1-{3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionyl}-pyrrolidine-2-carboxylic acid; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 118964-73-1,118964-75-3
1-[2-[2-(Naphthalene-2-sulfonylamino)-acetylamino]-3-(4-thiocarbamoyl-phenyl)-propionyl]-pyrrolidine-2-carboxylic acid

: 74-88-4
methyl iodide

: 118964-78-6,118964-80-0
1-{3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionyl}-pyrrolidine-2-carboxylic acid; hydriodide

Guidance literature:: In acetone; for 0.166667h; Heating;

Reference yield: 60.0%

: 118964-73-1,118964-75-3
1-[2-[2-(Naphthalene-2-sulfonylamino)-acetylamino]-3-(4-thiocarbamoyl-phenyl)-propionyl]-pyrrolidine-2-carboxylic acid

: 74-88-4
methyl iodide

: 118964-78-6,118964-80-0
1-{3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionyl}-pyrrolidine-2-carboxylic acid; hydriodide

Guidance literature:: In acetone; for 0.166667h; Heating;

Reference yield:

: 147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7
L-proline

: 118964-78-6,118964-80-0
1-{3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionyl}-pyrrolidine-2-carboxylic acid; hydriodide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 4-ethylmorpholine, isobutyl chloroformate; 2.) 4-ethylmorpholine / 1.) CHCl₃, 0 deg C, 15 min 2.) CHCl₃, 0 deg C, 30 min, then 60 min, room temperature

2: H₂S, TEA / pyridine / 72 h / Ambient temperature

3: 65 percent / acetone / 0.17 h / Heating

With N-ethylmorpholine;; TEA; hydrogen sulfide; isobutyl chloroformate; In pyridine; acetone;