PrCo((bis(thiophenyl)glyoxime-H)2(pyridine)

Base Information

Chemical Name:PrCo((bis(thiophenyl)glyoxime-H)2(pyridine)
CAS No.:1159404-41-7
Molecular Formula:C₃₆H₃₄CoN₅O₄S₄
Molecular Weight:787.954
Hs Code.:

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Chemical Property of PrCo((bis(thiophenyl)glyoxime-H)2(pyridine)

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Technology Process of PrCo((bis(thiophenyl)glyoxime-H)2(pyridine)

There total 1 articles about PrCo((bis(thiophenyl)glyoxime-H)2(pyridine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1159404-38-2
CoCl((bis(thiophenyl)glyoxime-H)2(pyridine)

: 1159404-41-7
PrCo((bis(thiophenyl)glyoxime-H)2(pyridine)

Guidance literature:: With NaOH; sodium borohydride; In ethanol; soln. of Co compd. in EtOH purged (N2, 10 min), cooled (0°C, stirring), aq. solns. of NaOH and NaBH4 added, soln. of propyl halide in EtOH added, mixt. stirred (0°C, 1 h), concd. under vac., poured intoH20 contg. some drops of pyridine; ppt. filtered off, washed with H2O and dried, column chromy. (silica gel, CH2Cl2); elem. anal.;
DOI:10.1021/om900065k