ethyl β<(1-oxo-3,4-dihydro-2H-isoquinolyl)amino>cynnamate

Base Information

Chemical Name:ethyl β<(1-oxo-3,4-dihydro-2H-isoquinolyl)amino>cynnamate
CAS No.:83391-31-5
Molecular Formula:C₂₀H₂₀N₂O₃
Molecular Weight:336.39
Hs Code.:

Synonyms:

Suppliers and Price of ethyl β<(1-oxo-3,4-dihydro-2H-isoquinolyl)amino>cynnamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl β<(1-oxo-3,4-dihydro-2H-isoquinolyl)amino>cynnamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl β<(1-oxo-3,4-dihydro-2H-isoquinolyl)amino>cynnamate

There total 1 articles about ethyl β<(1-oxo-3,4-dihydro-2H-isoquinolyl)amino>cynnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39113-01-4
2-amino-3,4-dihydro-1(2H)-isoquinolinone

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 83391-31-5
ethyl β<(1-oxo-3,4-dihydro-2H-isoquinolyl)amino>cynnamate

Guidance literature:: toluene-4-sulfonic acid; In benzene; for 1h; Heating;

Reference yield:

: 83391-31-5
ethyl β<(1-oxo-3,4-dihydro-2H-isoquinolyl)amino>cynnamate

: 61001-28-3
2-phenyl-5,6-dihydro-pyrazolo<5,1-a>isoquinoline-1-carboxylic acid

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; for 5h; Heating;

Reference yield:

: 83391-31-5
ethyl β<(1-oxo-3,4-dihydro-2H-isoquinolyl)amino>cynnamate

: 61001-51-2
1-bromomethyl-2-phenyl-5,6-dihydro-pyrazolo<5,1-a>isoquinoline hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: 18.3 g / potassium t-butoxide / 2-methyl-propan-2-ol / 5 h / Heating

2: 76 percent / potassium bicarbonate / N,N-dimethyl-acetamide / 15 h / Ambient temperature

3: 72 percent / LiAlH₄ / tetrahydrofuran / 1.) room temp., 4 h; 2.) reflux, 1 h

4: 4 g / hydrogen bromide / acetic acid / 21 h / 60 °C

With lithium aluminium tetrahydride; potassium tert-butylate; hydrogen bromide; potassium hydrogencarbonate; In tetrahydrofuran; N,N-dimethyl acetamide; acetic acid; tert-butyl alcohol;