2',3'-Di-O-acetyl-5'-deoxy-5'-adenosine

Base Information

Chemical Name:2',3'-Di-O-acetyl-5'-deoxy-5'-adenosine
CAS No.:121517-92-8
Molecular Formula:C₂₀H₂₁N₅O₆S
Molecular Weight:459.483
Hs Code.:

2',3'-Di-O-acetyl-5'-deoxy-5'-<phenylsulfinyl>adenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',3'-Di-O-acetyl-5'-deoxy-5'-adenosine

Chemical Property:

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Technology Process of 2',3'-Di-O-acetyl-5'-deoxy-5'-adenosine

There total 1 articles about 2',3'-Di-O-acetyl-5'-deoxy-5'-adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 149725-73-5
2',3'-Di-O-acetyl-5'-S-phenyl-5'-thioadenosine

: 121517-91-7,121517-92-8
2',3'-Di-O-acetyl-5'-deoxy-5'-adenosine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -40 ℃;
DOI:10.1016/S0040-4039(00)82174-7

Reference yield: 68.0%

: 121517-91-7,121517-92-8
2',3'-Di-O-acetyl-5'-deoxy-5'-adenosine

: 149725-73-5
2',3'-Di-O-acetyl-5'-S-phenyl-5'-thioadenosine

: 121517-93-9,121517-94-0
2',3'-Di-O-acetyl-5'-fluoro-5'-S-phenyl-5'-thioadenosine

Guidance literature:: With diethylamino-sulfur trifluoride; antimony(III) chloride; In dichloromethane; for 10h; Ambient temperature; var. Lewis acid catalysts;
DOI:10.1016/S0040-4039(00)82174-7

Reference yield:

: 121517-91-7,121517-92-8
2',3'-Di-O-acetyl-5'-deoxy-5'-adenosine

: (5'R)-2',3'-Di-O-acetyl-5'-fluoro-5'-S-phenyl-5'-thioadenosine

: (5'S)-2',3'-Di-O-acetyl-5'-fluoro-5'-S-phenyl-5'-thioadenosine

Guidance literature:: With (diethylamido)sulfur trifluoride; antimony(III) chloride; In dichloromethane; for 10h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo00082a010