Technology Process of 1,2-Benzenediol, 4-[2-(methylsulfonyl)ethyl]-
There total 4 articles about 1,2-Benzenediol, 4-[2-(methylsulfonyl)ethyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
N,N-dimethyl-formamide;
Ambient temperature;
DOI:10.1021/jm00384a038
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 77 percent / KOH / methanol / 2 h / Ambient temperature
2: 72 percent / CF3COOH, Et3SiH / CH2Cl2 / 7 h / Ambient temperature
3: 95 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h / 0 °C
4: 90 percent / m-chloroperbenzoic acid / dimethylformamide / Ambient temperature
With
triethylsilane; potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00384a038
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 72 percent / CF3COOH, Et3SiH / CH2Cl2 / 7 h / Ambient temperature
2: 95 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h / 0 °C
3: 90 percent / m-chloroperbenzoic acid / dimethylformamide / Ambient temperature
With
triethylsilane; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00384a038