phenoxy-[2,9,17-tri(tert-butyldimethylsilyloxy)-7,12:14,19-diimino-21,5-nitrilo-5H-tribenzo[c,h,m][1,6,11]triazacyclopentadecinato-(2)-κN(22),κN(23),κN(24)]-boron(III)

Base Information

Chemical Name:phenoxy-[2,9,17-tri(tert-butyldimethylsilyloxy)-7,12:14,19-diimino-21,5-nitrilo-5H-tribenzo[c,h,m][1,6,11]triazacyclopentadecinato-(2)-κN(22),κN(23),κN(24)]-boron(III)
CAS No.:1163700-08-0
Molecular Formula:C₄₈H₅₉BN₆O₄Si₃
Molecular Weight:879.102
Hs Code.:

phenoxy-[2,9,17-tri(tert-butyldimethylsilyloxy)-7,12:14,19-diimino-21,5-nitrilo-5H-tribenzo[c,h,m][1,6,11]triazacyclopentadecinato-(2)-κN(22),κN(23),κN(24)]-boron(III)

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Chemical Property of phenoxy-[2,9,17-tri(tert-butyldimethylsilyloxy)-7,12:14,19-diimino-21,5-nitrilo-5H-tribenzo[c,h,m][1,6,11]triazacyclopentadecinato-(2)-κN(22),κN(23),κN(24)]-boron(III)

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Technology Process of phenoxy-[2,9,17-tri(tert-butyldimethylsilyloxy)-7,12:14,19-diimino-21,5-nitrilo-5H-tribenzo[c,h,m][1,6,11]triazacyclopentadecinato-(2)-κN(22),κN(23),κN(24)]-boron(III)

There total 1 articles about phenoxy-[2,9,17-tri(tert-butyldimethylsilyloxy)-7,12:14,19-diimino-21,5-nitrilo-5H-tribenzo[c,h,m][1,6,11]triazacyclopentadecinato-(2)-κN(22),κN(23),κN(24)]-boron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1086965-15-2
4-(tert-butyldimethylsilyloxy)phthalonitrile

: 108-95-2,27073-41-2
phenol

: 1163700-09-1
phenoxy-[2,9,16-tri(tert-butyldimethylsilyloxy)-7,12:14,19-diimino-21,5-nitrilo-5H-tribenzo[c,h,m][1,6,11]triazacyclopentadecinato-(2)-κN(22),κN(23),κN(24)]-boron(III)

: 1163700-08-0
phenoxy-[2,9,17-tri(tert-butyldimethylsilyloxy)-7,12:14,19-diimino-21,5-nitrilo-5H-tribenzo[c,h,m][1,6,11]triazacyclopentadecinato-(2)-κN(22),κN(23),κN(24)]-boron(III)

Guidance literature:: 4-(tert-butyldimethylsilyloxy)phthalonitrile; With boron trichloride; In para-xylene; for 0.166667h; Inert atmosphere; Reflux;

phenol; In para-xylene; at 100 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.200801250