C₃₀H₄₈N₆O₃*6C₇H₈O₃S

Base Information

Chemical Name:C₃₀H₄₈N₆O₃*6C₇H₈O₃S
CAS No.:109774-86-9
Molecular Formula:6C₇H₈O₃S*C₃₀H₄₈N₆O₃
Molecular Weight:1573.98
Hs Code.:

C<sub>30</sub>H<sub>48</sub>N<sub>6</sub>O<sub>3</sub>*6C<sub>7</sub>H<sub>8</sub>O<sub>3</sub>S

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Chemical Property of C₃₀H₄₈N₆O₃*6C₇H₈O₃S

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Technology Process of C₃₀H₄₈N₆O₃*6C₇H₈O₃S

There total 8 articles about C₃₀H₄₈N₆O₃*6C₇H₈O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18226-42-1
1,3,5-Tris(bromomethyl)benzene

: 109774-86-9
C₃₀H₄₈N₆O₃*6C₇H₈O₃S

Guidance literature:: Multi-step reaction with 9 steps

1: sodium azide

2: LiAlH₄

4: 60 percent / K₂CO₃ / dimethylformamide / 36 h / 80 °C

5: 96 percent / MeOH / pTsOH / 1 h / Ambient temperature

6: 98 percent / Et₃N / CH₂Cl₂ / 2 h / -78 - 25 °C

7: 35 percent

8: 33percent HBr, phenol / acetic acid / 24 h / 40 °C

9: ionexchange resin (basic form)

With methanol; lithium aluminium tetrahydride; sodium azide; ionexchange resin (basic form); hydrogen bromide; potassium carbonate; triethylamine; phenol; toluene-4-sulfonic acid; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)85349-6

Reference yield:

: 77372-56-6
1,3,5-tris(aminomethyl)benzene

: 109774-86-9
C₃₀H₄₈N₆O₃*6C₇H₈O₃S

Guidance literature:: Multi-step reaction with 7 steps

2: 60 percent / K₂CO₃ / dimethylformamide / 36 h / 80 °C

3: 96 percent / MeOH / pTsOH / 1 h / Ambient temperature

4: 98 percent / Et₃N / CH₂Cl₂ / 2 h / -78 - 25 °C

5: 35 percent

6: 33percent HBr, phenol / acetic acid / 24 h / 40 °C

7: ionexchange resin (basic form)

With methanol; ionexchange resin (basic form); hydrogen bromide; potassium carbonate; triethylamine; phenol; toluene-4-sulfonic acid; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)85349-6

Reference yield:

: 109774-71-2
C₃₀H₃₃N₃O₆S₃

: 109774-86-9
C₃₀H₄₈N₆O₃*6C₇H₈O₃S

Guidance literature:: Multi-step reaction with 6 steps

1: 60 percent / K₂CO₃ / dimethylformamide / 36 h / 80 °C

2: 96 percent / MeOH / pTsOH / 1 h / Ambient temperature

3: 98 percent / Et₃N / CH₂Cl₂ / 2 h / -78 - 25 °C

4: 35 percent

5: 33percent HBr, phenol / acetic acid / 24 h / 40 °C

6: ionexchange resin (basic form)

With methanol; ionexchange resin (basic form); hydrogen bromide; potassium carbonate; triethylamine; phenol; toluene-4-sulfonic acid; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)85349-6