C₆₅H₁₁₆NO₁₇PSi₂

Base Information

Chemical Name:C₆₅H₁₁₆NO₁₇PSi₂
CAS No.:136358-65-1
Molecular Formula:C₆₅H₁₁₆NO₁₇PSi₂
Molecular Weight:1270.78
Hs Code.:

C<sub>65</sub>H<sub>116</sub>NO<sub>17</sub>PSi<sub>2</sub>

Synonyms:

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Chemical Property of C₆₅H₁₁₆NO₁₇PSi₂

Chemical Property:

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Technology Process of C₆₅H₁₁₆NO₁₇PSi₂

There total 19 articles about C₆₅H₁₁₆NO₁₇PSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 136358-65-1,136458-85-0
C₆₅H₁₁₆NO₁₇PSi₂

Guidance literature:: Multi-step reaction with 8 steps

1: 93 percent / 2,6-lutidine / CH₂Cl₂ / 0.25 h / -78 - 20 °C

2: 60.4 percent / dihydroquinidine acetate, OsO₄ / toluene / 5 h

3: 96 percent / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 2 h

4: 80 percent / 4A molecular sieves, camphorsulfonic acid / benzene; tetrahydrofuran / 2 h / Ambient temperature

5: 95 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.33 h

6: 90.8 percent / aq. LiOH / tetrahydrofuran; methanol / 2 h / -15 - -10 °C

7: N-metylmorpholine, (benzotriazolyl-1-oxy)tris(dimethylamino)phosphonium hexafluorophosphate (BOP) / CH₂Cl₂ / 3 h / Ambient temperature

8: 10percent aq. HCl / tetrahydrofuran / 0.08 h

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; lithium hydroxide; osmium(VIII) oxide; hydroquinidine acetate; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; dicyclohexyl-carbodiimide; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; benzene;

Reference yield:

: 136358-53-7,136358-54-8
<2R,S,3R,5S,6S,6(1S,2S)>-2-hydroxy-6-<2-(benzyloxy)-1-methoxy-3-methylbutyl>-5-methoxy-3-methyltetrahydropyran

: 136358-65-1,136458-85-0
C₆₅H₁₁₆NO₁₇PSi₂

Guidance literature:: Multi-step reaction with 9 steps

1: 73.5 percent / acetonitrile / 72 h / Heating

2: 93 percent / 2,6-lutidine / CH₂Cl₂ / 0.25 h / -78 - 20 °C

3: 60.4 percent / dihydroquinidine acetate, OsO₄ / toluene / 5 h

4: 96 percent / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 2 h

5: 80 percent / 4A molecular sieves, camphorsulfonic acid / benzene; tetrahydrofuran / 2 h / Ambient temperature

6: 95 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.33 h

7: 90.8 percent / aq. LiOH / tetrahydrofuran; methanol / 2 h / -15 - -10 °C

8: N-metylmorpholine, (benzotriazolyl-1-oxy)tris(dimethylamino)phosphonium hexafluorophosphate (BOP) / CH₂Cl₂ / 3 h / Ambient temperature

9: 10percent aq. HCl / tetrahydrofuran / 0.08 h

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; lithium hydroxide; osmium(VIII) oxide; hydroquinidine acetate; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; dicyclohexyl-carbodiimide; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; acetonitrile; benzene;

Reference yield:

: 136358-37-7
(2E,6S,7S,8R,9S)-7-hydroxy-6,8-dimethoxy-4,10-dimethyl-9-(phenylmethoxy)-2-undecenoic acid methyl ester

: 136358-65-1,136458-85-0
C₆₅H₁₁₆NO₁₇PSi₂

Guidance literature:: Multi-step reaction with 8 steps

1: 93 percent / 2,6-lutidine / CH₂Cl₂ / 0.25 h / -78 - 20 °C

2: 60.4 percent / dihydroquinidine acetate, OsO₄ / toluene / 5 h

3: 96 percent / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 2 h

4: 80 percent / 4A molecular sieves, camphorsulfonic acid / benzene; tetrahydrofuran / 2 h / Ambient temperature

5: 95 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.33 h

6: 90.8 percent / aq. LiOH / tetrahydrofuran; methanol / 2 h / -15 - -10 °C

7: N-metylmorpholine, (benzotriazolyl-1-oxy)tris(dimethylamino)phosphonium hexafluorophosphate (BOP) / CH₂Cl₂ / 3 h / Ambient temperature

8: 10percent aq. HCl / tetrahydrofuran / 0.08 h

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; lithium hydroxide; osmium(VIII) oxide; hydroquinidine acetate; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; dicyclohexyl-carbodiimide; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; benzene;