C₁₄H₂₃NO

Base Information

Chemical Name:C₁₄H₂₃NO
CAS No.:1359985-30-0
Molecular Formula:C₁₄H₂₃NO
Molecular Weight:221.343
Hs Code.:

Synonyms:

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Chemical Property of C₁₄H₂₃NO

Chemical Property:

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Technology Process of C₁₄H₂₃NO

There total 11 articles about C₁₄H₂₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₆O₄

: 1359985-30-0
C₁₄H₂₃NO

Guidance literature:: Multi-step reaction with 9 steps

1: diphenyl phosphoryl azide; triethylamine / toluene / 1 h / 70 °C

2: triethylamine / toluene / 5 h / 80 °C

3: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 5 h / 20 °C

4: borane-THF / tetrahydrofuran / 4 h / -5 °C

5: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

6: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

7: acetic acid / toluene / 2 h / Reflux

8: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

9: diethyl ether / 0.5 h / 0 °C

With tetrapropylammonium perruthennate; borane-THF; lithium hydroxide monohydrate; diphenyl phosphoryl azide; palladium 10% on activated carbon; water; hydrogen; acetic acid; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; carbon dioxide; toluene; 2: Curtius rearrangement / 9: Grignard reaction;
DOI:10.1055/s-0031-1289884

Reference yield:

: C₁₀H₁₅N₃O₃

: 1359985-30-0
C₁₄H₂₃NO

Guidance literature:: Multi-step reaction with 8 steps

1: triethylamine / toluene / 5 h / 80 °C

2: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 5 h / 20 °C

3: borane-THF / tetrahydrofuran / 4 h / -5 °C

4: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

5: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

6: acetic acid / toluene / 2 h / Reflux

7: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

8: diethyl ether / 0.5 h / 0 °C

With tetrapropylammonium perruthennate; borane-THF; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; acetic acid; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; carbon dioxide; toluene; 1: Curtius rearrangement / 8: Grignard reaction;
DOI:10.1055/s-0031-1289884

Reference yield:

: 952616-39-6
C₁₅H₁₉NO₄

: 1359985-30-0
C₁₄H₂₃NO

Guidance literature:: Multi-step reaction with 6 steps

1: borane-THF / tetrahydrofuran / 4 h / -5 °C

2: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

3: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

4: acetic acid / toluene / 2 h / Reflux

5: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

6: diethyl ether / 0.5 h / 0 °C

With tetrapropylammonium perruthennate; borane-THF; palladium 10% on activated carbon; hydrogen; acetic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; carbon dioxide; toluene; 6: Grignard reaction;
DOI:10.1055/s-0031-1289884