dimesityl-di(t-butylimido)molybdenum(VI)

Base Information

Chemical Name:dimesityl-di(t-butylimido)molybdenum(VI)
CAS No.:116881-11-9
Molecular Formula:C₂₆H₄₀MoN₂
Molecular Weight:476.557
Hs Code.:

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Chemical Property of dimesityl-di(t-butylimido)molybdenum(VI)

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Technology Process of dimesityl-di(t-butylimido)molybdenum(VI)

There total 1 articles about dimesityl-di(t-butylimido)molybdenum(VI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 71851-95-1
bis(tert-butylimido)bis(trimethylsiloxo)molybdenum

: 2633-66-1
2-mesitylmagnesium bromide

: 135912-59-3
Br^(1-)*C₃H₉OSi^(1-)*Mg⁽²⁺⁾

: 116881-11-9
dimesityl-di(t-butylimido)molybdenum(VI)

Guidance literature:: In diethyl ether; hexane; to a stirred soln. of the Mo compound in hexane is added the Grignard reagent in Et2O at room temp.; mixt. stirred for 2 h; solvent removed in vac., residue extd. with hexane; filtration, concn., cooling to -21°C yields crystals; elem. anal.;
DOI:10.1039/DT9880000053

Reference yield: 92.0%

: 116881-11-9
dimesityl-di(t-butylimido)molybdenum(VI)

: 103-71-9
phenyl isocyanate

: t-butyl-mesitylamine

: 5215-40-7
2,4,6-trimethyl-N-phenylbenzamide

: 1785-02-0
triphenyl isocyanurate

Guidance literature:: In not given; under oxygen-free N2, cooling at -30°C, PhNCO added, warmed slowly to room temperature, stirred 5 h;
DOI:10.1016/S0277-5387(00)80213-2

Reference yield: 91.0%

: 148-24-3,24804-14-6
8-quinolinol

: 116881-11-9
dimesityl-di(t-butylimido)molybdenum(VI)

: bis(tert-butylimido)(2,4,6-trimethylphenyl)(8-oxyquinolinato)molybdenum

Guidance literature:: In hexane; organomolybdenum compd. and 8-hydroxyquinoline are dissolved in hexane under argon, mixt. is stirred overnight; filtn., evapn. (vac.), washing (hexane); elem. anal.;