C₇₁H₇₃NO₄S

Base Information

• Chemical Name: C₇₁H₇₃NO₄S
• CAS No.: 1384183-23-6
• Molecular Formula: C₇₁H₇₃NO₄S
• Molecular Weight: 1036.43
• Mol file: 1384183-23-6.mol

Synonyms:

Chemical Property of C₇₁H₇₃NO₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₇₁H₇₃NO₄S

There total 1 articles about C₇₁H₇₃NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C64H69NO3S (1376156-93-2) + 4-bromo-benzaldehyde (1122-91-4) → C71H73NO4S (1384183-23-6)

Guidance literature:

C₆₄H₆₉NO₃S; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

With tributyltin chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

4-bromo-benzaldehyde; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 4h; Reflux; Inert atmosphere;

DOI:10.1039/c2cc32926c

Reference yield: 93.9%

C71H73NO4S (1384183-23-6) + cyanoacetic acid (372-09-8) → C74H74N2O5S (1384183-28-1)

Guidance literature:

With piperidine; In chloroform; acetonitrile; for 5h; Reflux;

DOI:10.1039/c2cc32926c

upstream raw materials:

C₆₄H₆₉NO₃S

4-bromo-benzaldehyde

Downstream raw materials:

C₇₄H₇₄N₂O₅S