C₁₄H₁₃NO₅

Base Information

Chemical Name:C₁₄H₁₃NO₅
CAS No.:1202802-49-0
Molecular Formula:C₁₄H₁₃NO₅
Molecular Weight:275.261
Hs Code.:

C<sub>14</sub>H<sub>13</sub>NO<sub>5</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₃NO₅

Chemical Property:

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Technology Process of C₁₄H₁₃NO₅

There total 7 articles about C₁₄H₁₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1202802-95-6
1-(4-((benzyloxy)carbonyl)-3-hydroxyphenyl)-2,5-dimethyl-1H-pyrrole-3-carboxylic acid

: 1202802-49-0
C₁₄H₁₃NO₅

Guidance literature:: With hydrogen fluoride; at 0 ℃; for 1h;
DOI:10.1021/jm3018964

Reference yield:

: 318511-70-5
tert-butyl 2-acetyl-4-oxopentanoate

: 1202802-49-0
C₁₄H₁₃NO₅

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methyl-morpholine; toluene-4-sulfonic acid / toluene / 3 h / Reflux

2: hydrogenchloride / ethyl acetate / 1 h / 20 °C

3: hydrogen fluoride / 1 h / 0 °C

With 4-methyl-morpholine; hydrogenchloride; hydrogen fluoride; toluene-4-sulfonic acid; In ethyl acetate; toluene;
DOI:10.1021/jm3018964

Reference yield:

: 65-49-6
4-Aminosalicylic acid

: 1202802-49-0
C₁₄H₁₃NO₅

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / 1,4-dioxane; water / 2 h / 20 °C / Cooling with ice

2: dicyclohexyl-carbodiimide; dmap / dichloromethane; N,N-dimethyl-formamide / Reflux

3: hydrogenchloride / ethyl acetate / 2 h / 20 °C

4: 4-methyl-morpholine; toluene-4-sulfonic acid / toluene / 3 h / Reflux

5: hydrogenchloride / ethyl acetate / 1 h / 20 °C

6: hydrogen fluoride / 1 h / 0 °C

With 4-methyl-morpholine; hydrogenchloride; dmap; hydrogen fluoride; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; sodium hydroxide; In 1,4-dioxane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm3018964