C₁₂H₁₈O₂

Base Information

Chemical Name:C₁₂H₁₈O₂
CAS No.:1412901-91-7
Molecular Formula:C₁₂H₁₈O₂
Molecular Weight:194.274
Hs Code.:

C<sub>12</sub>H<sub>18</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₈O₂

Chemical Property:

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Technology Process of C₁₂H₁₈O₂

There total 3 articles about C₁₂H₁₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 132587-07-6,132587-15-6,2833-34-3
1-phenylbut-3-enyl acetate

: 346713-20-0
allylsamarium bromide

: 1412901-91-7
C₁₂H₁₈O₂

: 2-(2-hydroxy-2-phenylethyl)-1-methylcyclopropanol

: 2-(2-hydroxy-2-phenylethyl)-1-methylcyclopropanol

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; water; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c2cc34630c

Reference yield:

: 100-52-7
benzaldehyde

: 1412901-91-7
C₁₂H₁₈O₂

: 2-(2-hydroxy-2-phenylethyl)-1-methylcyclopropanol

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium chloride; zinc / tetrahydrofuran; water / 20 °C

2: pyridine / dichloromethane / 24 h / 34 - 37 °C

3: N,N,N,N,N,N-hexamethylphosphoric triamide; water / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; water; ammonium chloride; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c2cc34630c

Reference yield:

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 1412901-91-7
C₁₂H₁₈O₂

: 2-(2-hydroxy-2-phenylethyl)-1-methylcyclopropanol

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 24 h / 34 - 37 °C

2: N,N,N,N,N,N-hexamethylphosphoric triamide; water / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; water; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2cc34630c