(2R,3R)-methyl 3-nitro-2-phenylpentanoate

Base Information

Chemical Name:(2R,3R)-methyl 3-nitro-2-phenylpentanoate
CAS No.:1444826-67-8
Molecular Formula:C₁₂H₁₅NO₄
Molecular Weight:237.255
Hs Code.:

Synonyms:

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Chemical Property of (2R,3R)-methyl 3-nitro-2-phenylpentanoate

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Technology Process of (2R,3R)-methyl 3-nitro-2-phenylpentanoate

There total 4 articles about (2R,3R)-methyl 3-nitro-2-phenylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85217-69-2,87802-71-9
cinnamyl methyl carbonate

: 1444826-67-8
(2R,3R)-methyl 3-nitro-2-phenylpentanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: C₄₀H₄₁FeN₂O₃P; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,4-diaza-bicyclo[2.2.2]octane / tetrahydrofuran; dimethyl sulfoxide / 0 °C / Inert atmosphere

2.1: ozone / dichloromethane / -78 °C

2.2: -78 - 20 °C

3.1: sodium dihydrogenphosphate dihydrate; sodium chlorite; 2-methyl-but-2-ene / tert-butyl alcohol; water / 2 h / 0 °C

4.1: dmap; dicyclohexyl-carbodiimide / 0 - 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; C₄₀H₄₁FeN₂O₃P; ozone; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1021/jo400663d

Reference yield:

: C₁₁H₁₃NO₃

: 1444826-67-8
(2R,3R)-methyl 3-nitro-2-phenylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium dihydrogenphosphate dihydrate; sodium chlorite; 2-methyl-but-2-ene / tert-butyl alcohol; water / 2 h / 0 °C

2: dmap; dicyclohexyl-carbodiimide / 0 - 20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; dicyclohexyl-carbodiimide; In water; tert-butyl alcohol;
DOI:10.1021/jo400663d

Reference yield:

: 1444826-32-7
(3R,4R)-(4-nitrohex-1-en-3-yl)benzene

: 1444826-67-8
(2R,3R)-methyl 3-nitro-2-phenylpentanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ozone / dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: sodium dihydrogenphosphate dihydrate; sodium chlorite; 2-methyl-but-2-ene / tert-butyl alcohol; water / 2 h / 0 °C

3.1: dmap; dicyclohexyl-carbodiimide / 0 - 20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; ozone; dicyclohexyl-carbodiimide; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jo400663d