(eta.4-1,5-cycloocatadiene)[α-phenyl-(2-pyridinemethanimine)-N,N']rhodium hexafluorophosphate

Base Information

Chemical Name:(eta.4-1,5-cycloocatadiene)[α-phenyl-(2-pyridinemethanimine)-N,N']rhodium hexafluorophosphate
CAS No.:90478-87-8
Molecular Formula:C₂₀H₂₂N₂Rh*F₆P
Molecular Weight:538.278
Hs Code.:

Synonyms:

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Chemical Property of (eta.4-1,5-cycloocatadiene)[α-phenyl-(2-pyridinemethanimine)-N,N']rhodium hexafluorophosphate

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Technology Process of (eta.4-1,5-cycloocatadiene)[α-phenyl-(2-pyridinemethanimine)-N,N']rhodium hexafluorophosphate

There total 2 articles about (eta.4-1,5-cycloocatadiene)[α-phenyl-(2-pyridinemethanimine)-N,N']rhodium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: ammonium hexafluorophosphate

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: (3R)-N-(phenyl-2-pyridinylmethylene)-3-pinanemethanamine

: 90478-87-8
(eta.4-1,5-cycloocatadiene)[α-phenyl-(2-pyridinemethanimine)-N,N']rhodium hexafluorophosphate

Guidance literature:: In methanol; stirring the 2 soln. with the ligand for 5 min, then adding NH4PF6 to the soln. and stirring for 30 min; after evapn. of the solvent the residue was solved in CH2Cl2/ether, theunsolved salt was filtered, chromy., recrystn. from methanol, elem. anal.;

Reference yield: 95.0%

: ammonium hexafluorophosphate

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 81643-05-2
(S)-α-methyl-N-(phenyl-2-pyridinylmethylene)benzenemethanamine

: 90478-87-8
(eta.4-1,5-cycloocatadiene)[α-phenyl-(2-pyridinemethanimine)-N,N']rhodium hexafluorophosphate

Guidance literature:: In methanol; stirring the 2 soln. with the ligand for 5 min, then adding NH4PF6 to the soln. and stirring for 30 min; after evapn. of the solvent the residue was solved in CH2Cl2/ether, theunsolved salt was filtered, chromy., recrystn. from methanol, elem. anal.;