2-<2-(α-Hydroxybenzyl)-phenyl>-acetaldehydethylenacetal

Base Information

Chemical Name:2-<2-(α-Hydroxybenzyl)-phenyl>-acetaldehydethylenacetal
CAS No.:130089-30-4
Molecular Formula:C₁₇H₁₈O₃
Molecular Weight:270.328
Hs Code.:

Synonyms:

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Chemical Property of 2-<2-(α-Hydroxybenzyl)-phenyl>-acetaldehydethylenacetal

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Technology Process of 2-<2-(α-Hydroxybenzyl)-phenyl>-acetaldehydethylenacetal

There total 5 articles about 2-<2-(α-Hydroxybenzyl)-phenyl>-acetaldehydethylenacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 130089-30-4
2-<2-(α-Hydroxybenzyl)-phenyl>-acetaldehydethylenacetal

Guidance literature:: Multi-step reaction with 5 steps

1: 90.6 percent / NaOMe / methanol / 1.) 1 h, -10 deg C, 2.) 16 h, room temperature

2: 86.4 percent / aq. KOH / ethanol / 1 h

3: 52.4 percent / Heating

4: 76.7 percent / p-TsOH / benzene / 4 h / Heating

5: 1.) n-BuLi / 1.) THF, hexane, -82 deg C, 1 h, 2.) THF, 2 h

With potassium hydroxide; n-butyllithium; sodium methylate; toluene-4-sulfonic acid; In methanol; ethanol; benzene;
DOI:10.1002/ardp.19903230810

Reference yield:

: 96557-30-1
2-bromophenylacetaldehyde

: 130089-30-4
2-<2-(α-Hydroxybenzyl)-phenyl>-acetaldehydethylenacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 76.7 percent / p-TsOH / benzene / 4 h / Heating

2: 1.) n-BuLi / 1.) THF, hexane, -82 deg C, 1 h, 2.) THF, 2 h

With n-butyllithium; toluene-4-sulfonic acid; In benzene;
DOI:10.1002/ardp.19903230810

Reference yield:

: 130089-22-4
3-(2-Bromphenyl)-2-oxirancarbonsaeure

: 130089-30-4
2-<2-(α-Hydroxybenzyl)-phenyl>-acetaldehydethylenacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 52.4 percent / Heating

2: 76.7 percent / p-TsOH / benzene / 4 h / Heating

3: 1.) n-BuLi / 1.) THF, hexane, -82 deg C, 1 h, 2.) THF, 2 h

With n-butyllithium; toluene-4-sulfonic acid; In benzene;
DOI:10.1002/ardp.19903230810