(C₆H₅)3CSC₄H₆NCO₂CH₂CHCH₂CNOCH₃CH₂NHSO₂NHCH₂CH₃

Base Information

Chemical Name:(C₆H₅)3CSC₄H₆NCO₂CH₂CHCH₂CNOCH₃CH₂NHSO₂NHCH₂CH₃
CAS No.:936213-89-7
Molecular Formula:C₃₂H₃₈N₄O₅S₂
Molecular Weight:622.81
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>)3CSC<sub>4</sub>H<sub>6</sub>NCO<sub>2</sub>CH<sub>2</sub>CHCH<sub>2</sub>CNOCH<sub>3</sub>CH<sub>2</sub>NHSO<sub>2</sub>NHCH<sub>2</sub>CH<sub>3</sub>

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Chemical Property of (C₆H₅)3CSC₄H₆NCO₂CH₂CHCH₂CNOCH₃CH₂NHSO₂NHCH₂CH₃

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Technology Process of (C₆H₅)3CSC₄H₆NCO₂CH₂CHCH₂CNOCH₃CH₂NHSO₂NHCH₂CH₃

There total 4 articles about (C₆H₅)3CSC₄H₆NCO₂CH₂CHCH₂CNOCH₃CH₂NHSO₂NHCH₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (C₆H₅)3CSC₄H₆NCO₂CH₂CHCH₂CNOCH₃CH₂NH₂*HCl

: 16548-07-5
ethylsulfamoyl chloride

: 936213-89-7
(C₆H₅)3CSC₄H₆NCO₂CH₂CHCH₂CNOCH₃CH₂NHSO₂NHCH₂CH₃

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.ejmech.2006.10.006

Reference yield:

: 894433-05-7
(2S,4S)-2-[(1-oxo-2-nitro)ethyl]-4-tritylthio-1-(allyloxycarbonyl)pyrrolidine

: 936213-89-7
(C₆H₅)3CSC₄H₆NCO₂CH₂CHCH₂CNOCH₃CH₂NHSO₂NHCH₂CH₃

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / pyridine / 10 h / 50 °C

2: indium; aq. HCl / tetrahydrofuran / 4 h / 20 °C

3: triethylamine / CH₂Cl₂ / 1 h / 0 °C

With pyridine; hydrogenchloride; indium; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2006.10.006

Reference yield:

: 894433-08-0
(2S,4S)-2-(1-methoxyimino-2-nitroethyl)-4-tritylthio-1-(allyloxycarbonyl)pyrrolidine

: 936213-89-7
(C₆H₅)3CSC₄H₆NCO₂CH₂CHCH₂CNOCH₃CH₂NHSO₂NHCH₂CH₃

Guidance literature:: Multi-step reaction with 2 steps

1: indium; aq. HCl / tetrahydrofuran / 4 h / 20 °C

2: triethylamine / CH₂Cl₂ / 1 h / 0 °C

With hydrogenchloride; indium; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2006.10.006