(3'R)-1'-acetyl-4't-anilino-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinoline]

Base Information

• Chemical Name: (3'R)-1'-acetyl-4't-anilino-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinoline]
• CAS No.: 21286-53-3
• Molecular Formula: C₂₆H₃₂N₂O₅
• Molecular Weight: 452.55

Synonyms:

Chemical Property of (3'R)-1'-acetyl-4't-anilino-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinoline]

Chemical Property:

Purity/Quality:

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Technology Process of (3'R)-1'-acetyl-4't-anilino-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinoline]

There total 3 articles about (3'R)-1'-acetyl-4't-anilino-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinoline] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aniline (62-53-3) → (3'R)-1'-acetyl-4't-anilino-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinoline] (21286-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid

2: Py

With pyridine; In acetic acid;

DOI:10.1246/bcsj.41.2735

Reference yield:

(4S)-2,2-dimethyl-[1,3]dioxolane-4-carbaldehyde (22323-80-4) → (3'R)-1'-acetyl-4't-anilino-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinoline] (21286-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid

2: Py

With pyridine; In acetic acid;

DOI:10.1246/bcsj.41.2735

Reference yield:

[(3'R)-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinolin]-4't-yl]-phenyl-amine (21400-69-1) + acetyl chloride (75-36-5) → (3'R)-1'-acetyl-4't-anilino-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinoline] (21286-53-3)

Guidance literature:

With pyridine;

DOI:10.1246/bcsj.41.2735

upstream raw materials:

[(3'R)-2't-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-1',4'-dihydro-2'H-(3'rO)-spiro[[1,3]dioxolane-4,3'-quinolin]-4't-yl]-phenyl-amine

acetyl chloride

aniline

(4S)-2,2-dimethyl-[1,3]dioxolane-4-carbaldehyde

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