Phosphonium, [2-(2-methyl-1,3-dioxolan-2-yl)-1-methylenepropyl]triphenyl-, iodide

Base Information

Chemical Name:Phosphonium, [2-(2-methyl-1,3-dioxolan-2-yl)-1-methylenepropyl]triphenyl-, iodide
CAS No.:104803-69-2
Molecular Formula:C₂₆H₂₈O₂P*I
Molecular Weight:530.385
Hs Code.:
Mol file:104803-69-2.mol

Synonyms:

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Chemical Property of Phosphonium, [2-(2-methyl-1,3-dioxolan-2-yl)-1-methylenepropyl]triphenyl-, iodide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phosphonium, [2-(2-methyl-1,3-dioxolan-2-yl)-1-methylenepropyl]triphenyl-, iodide

There total 12 articles about Phosphonium, [2-(2-methyl-1,3-dioxolan-2-yl)-1-methylenepropyl]triphenyl-, iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82777-75-1
1-<(2-Methyl-1,3-dioxolan-2-yl)methyl>ethenyltriphenylphosphonium iodide

: 104803-69-2
iodure d'ethylenedioxy-2,2 methyl-3 pentene-4 yl-4 triphenylphosphonium

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / n-butyllithium / hexane; methanol / 4 h / Heating

2: 95 percent / 0.05N H₂SO₄ / H₂O / 5 h / 50 °C

3: triethylamine / methanol / 1 h / 20 °C

4: 1.) p-toluenesulfonic acid; 2.) p-toluenesulfonic acid, NaI/H₂O / 1.) chloroform, 0 --> 20 deg C, 1 h; 2.) chloroform, reflux, 12 h

With n-butyllithium; sulfuric acid; water; toluene-4-sulfonic acid; triethylamine; sodium iodide; In methanol; hexane; water;

Reference yield:

: 82777-74-0
iodure d'oxo-2 pentene-4 yl-4 triphenylphosphonium

: 104803-69-2
iodure d'ethylenedioxy-2,2 methyl-3 pentene-4 yl-4 triphenylphosphonium

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / p-toluenesulfonic acid / CHCl₃ / 19 h / Heating

2: 95 percent / n-butyllithium / hexane; methanol / 4 h / Heating

3: 95 percent / 0.05N H₂SO₄ / H₂O / 5 h / 50 °C

4: triethylamine / methanol / 1 h / 20 °C

5: 1.) p-toluenesulfonic acid; 2.) p-toluenesulfonic acid, NaI/H₂O / 1.) chloroform, 0 --> 20 deg C, 1 h; 2.) chloroform, reflux, 12 h

With n-butyllithium; sulfuric acid; water; toluene-4-sulfonic acid; triethylamine; sodium iodide; In methanol; hexane; chloroform; water;

Reference yield:

: 104803-74-9
iodure d'oxo-2 (hydroxy-2' ethoxy)-5 pentyl-4 triphenylphosphonium

: 104803-69-2
iodure d'ethylenedioxy-2,2 methyl-3 pentene-4 yl-4 triphenylphosphonium

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetonitrile / -15 deg C, 1h, then 20 deg C, 2 h, then 50 deg C, 12 h

2: 1.) p-toluenesulfonic acid; 2.) p-toluenesulfonic acid, NaI/H₂O / 1.) chloroform, 0 --> 20 deg C, 1 h; 2.) chloroform, reflux, 12 h

With water; toluene-4-sulfonic acid; triethylamine; sodium iodide; In acetonitrile;