3-Cyclopenten-1-one, 3-(2-phenylethyl)-

Base Information

Chemical Name:3-Cyclopenten-1-one, 3-(2-phenylethyl)-
CAS No.:104804-90-2
Molecular Formula:C₁₃H₁₄O
Molecular Weight:186.254
Hs Code.:
Mol file:104804-90-2.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Cyclopenten-1-one, 3-(2-phenylethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Cyclopenten-1-one, 3-(2-phenylethyl)-

There total 6 articles about 3-Cyclopenten-1-one, 3-(2-phenylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57242-69-0
2,3-dihydro-4H-thiopyran-4-one

: 104804-90-2
3-(2-phenylethyl)-3-cyclopentenone

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / 12 N aq. HCl / ethanol / 5 h / Ambient temperature

2: p-toluenesulfonic acid / benzene / 4 h / Heating

3: m-chloroperbenzoic acid / CH₂Cl₂ / 1.) 0 deg C, 1 h, 2). RT, 4 h

4: 1.) sodium hydride / 1.) DMF, RT, 0.5 h, 2.) DMF, a) RT, 39 h, b) 70 deg C, 6 h

5: 70 percent / sodium hydride, potassium hydride / dimethylsulfoxide / 48 h / Ambient temperature

6: pyridinium p-toluenesulfonate, water / acetone / 10 h / Heating

With hydrogenchloride; water; pyridinium p-toluenesulfonate; potassium hydride; sodium hydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; dimethyl sulfoxide; acetone; benzene;
DOI:10.1021/jo00385a011

Reference yield:

: 104804-78-6
2-(p-tolylsulfonyl)-4-thianone

: 104804-90-2
3-(2-phenylethyl)-3-cyclopentenone

Guidance literature:: Multi-step reaction with 5 steps

1: p-toluenesulfonic acid / benzene / 4 h / Heating

2: m-chloroperbenzoic acid / CH₂Cl₂ / 1.) 0 deg C, 1 h, 2). RT, 4 h

3: 1.) sodium hydride / 1.) DMF, RT, 0.5 h, 2.) DMF, a) RT, 39 h, b) 70 deg C, 6 h

4: 70 percent / sodium hydride, potassium hydride / dimethylsulfoxide / 48 h / Ambient temperature

5: pyridinium p-toluenesulfonate, water / acetone / 10 h / Heating

With water; pyridinium p-toluenesulfonate; potassium hydride; sodium hydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; dimethyl sulfoxide; acetone; benzene;
DOI:10.1021/jo00385a011

Reference yield:

: 104804-85-5
7-(2-phenylethyl)-7-(p-tolylsulfonyl)-1,4-dioxa-8-thiaspiro<4.5>-decane 8,8-dioxide

: 104804-90-2
3-(2-phenylethyl)-3-cyclopentenone

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / sodium hydride, potassium hydride / dimethylsulfoxide / 48 h / Ambient temperature

2: pyridinium p-toluenesulfonate, water / acetone / 10 h / Heating

With water; pyridinium p-toluenesulfonate; potassium hydride; sodium hydride; In dimethyl sulfoxide; acetone;
DOI:10.1021/jo00385a011