[(Au(tris(p-tolyl)phosphine))(3,5-diethynylpyridine(-2H))(Au(tris(p-tolyl)phosphine))2]TfO

Base Information

Chemical Name:[(Au(tris(p-tolyl)phosphine))(3,5-diethynylpyridine(-2H))(Au(tris(p-tolyl)phosphine))2]TfO
CAS No.:807619-46-1
Molecular Formula:CF₃O₃S*C₇₂H₆₆Au₃NP₃
Molecular Weight:1778.21
Hs Code.:

Synonyms:

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Chemical Property of [(Au(tris(p-tolyl)phosphine))(3,5-diethynylpyridine(-2H))(Au(tris(p-tolyl)phosphine))2]TfO

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Technology Process of [(Au(tris(p-tolyl)phosphine))(3,5-diethynylpyridine(-2H))(Au(tris(p-tolyl)phosphine))2]TfO

There total 4 articles about [(Au(tris(p-tolyl)phosphine))(3,5-diethynylpyridine(-2H))(Au(tris(p-tolyl)phosphine))2]TfO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 28978-10-1
(tri-p-tolylphosphine)gold(I) chloride

: 807619-42-7
[(Au(tris(p-tolyl)phosphine))2(μ-3,5-diethynylpyridine(-2H))]

: 73491-36-8
thallium(I) triflate

: 807619-46-1
[(Au(tris(p-tolyl)phosphine))(3,5-diethynylpyridine(-2H))(Au(tris(p-tolyl)phosphine))2]TfO

Guidance literature:: In tetrahydrofuran; byproducts: TlCl; stirred under N2 for 0.5 h; evapd. (vac.), stirred with CHCl3, filtered (Celite), evapd., stirred with n-pentane, filtered, air-dried; elem. anal.;
DOI:10.1021/om049509j

Reference yield:

: 67227-90-1
3,5-diethynyl pyridine

: 807619-46-1
[(Au(tris(p-tolyl)phosphine))(3,5-diethynylpyridine(-2H))(Au(tris(p-tolyl)phosphine))2]TfO

Guidance literature:: Multi-step reaction with 3 steps

1: (C₂H₅)3N / dichloromethane

2: dichloromethane

3: tetrahydrofuran

With (C₂H₅)3N; In tetrahydrofuran; dichloromethane;
DOI:10.1021/om049509j

Reference yield:

: [Au₂(3,5-diethynylpyridine(-2H)](n)

: 1038-95-5,218281-19-7
Tri(p-tolyl)phosphine

: 807619-46-1
[(Au(tris(p-tolyl)phosphine))(3,5-diethynylpyridine(-2H))(Au(tris(p-tolyl)phosphine))2]TfO

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: tetrahydrofuran

In tetrahydrofuran; dichloromethane;
DOI:10.1021/om049509j