11-deoxy-16-(3-methoxymethyl)phenyl-ω-tetranor-5-thiaPGE1

Base Information

Chemical Name:11-deoxy-16-(3-methoxymethyl)phenyl-ω-tetranor-5-thiaPGE1
CAS No.:256382-30-6
Molecular Formula:C₂₃H₃₂O₅S
Molecular Weight:420.57
Hs Code.:

Synonyms:

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Chemical Property of 11-deoxy-16-(3-methoxymethyl)phenyl-ω-tetranor-5-thiaPGE1

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Technology Process of 11-deoxy-16-(3-methoxymethyl)phenyl-ω-tetranor-5-thiaPGE1

There total 3 articles about 11-deoxy-16-(3-methoxymethyl)phenyl-ω-tetranor-5-thiaPGE1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 256382-18-0
11-deoxy-16-(3-methoxymethyl)phenyl-ω-tetranor-5-thiaPGE1 methyl ester

: 256382-30-6
11-deoxy-16-(3-methoxymethyl)phenyl-ω-tetranor-5-thiaPGE1

Guidance literature:: In ethanol; at 20 ℃; for 2h; pH=7.4; aq. phosphate buffer; Enzymatic reaction;
DOI:10.1248/cpb.59.1494

Reference yield:

: 443987-99-3
C₂₄H₃₂O₅S

: 256382-30-6
11-deoxy-16-(3-methoxymethyl)phenyl-ω-tetranor-5-thiaPGE1

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; lithium aluminium tetrahydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -78 °C / Inert atmosphere

2: ethanol / 2 h / 20 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction

With copper(l) iodide; lithium aluminium tetrahydride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol;
DOI:10.1248/cpb.59.1494

Reference yield:

: 256382-08-8
Rivenprost

: 256382-30-6
11-deoxy-16-(3-methoxymethyl)phenyl-ω-tetranor-5-thiaPGE1

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; acetic acid / water / 5 h / 80 °C / Inert atmosphere

2: copper(l) iodide; lithium aluminium tetrahydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -78 °C / Inert atmosphere

3: ethanol / 2 h / 20 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction

With hydrogenchloride; copper(l) iodide; lithium aluminium tetrahydride; acetic acid; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; water;
DOI:10.1248/cpb.59.1494