C₆H₄(CH₂)3BHN(CH₃)2CCH₃

Base Information

Chemical Name:C₆H₄(CH₂)3BHN(CH₃)2CCH₃
CAS No.:1350465-80-3
Molecular Formula:C₁₃H₂₀BN
Molecular Weight:201.12
Hs Code.:

C<sub>6</sub>H<sub>4</sub>(CH<sub>2</sub>)3BHN(CH<sub>3</sub>)2CCH<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆H₄(CH₂)3BHN(CH₃)2CCH₃

Chemical Property:

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Technology Process of C₆H₄(CH₂)3BHN(CH₃)2CCH₃

There total 4 articles about C₆H₄(CH₂)3BHN(CH₃)2CCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350465-78-9
C₆H₅CH₂C(CH₃)2CH₂N(CH₃)2BH₃

: 1350465-82-5
1,1,4,4-tetramethyl-3-phenyl-1,2-azaborolidine

: 1350465-79-0
4-benzyl-1,1,4-trimethyl-1,2-azaborolidine

: 1350465-80-3
C₆H₄(CH₂)3BHN(CH₃)2CCH₃

Guidance literature:: C₆H₅CH₂C(CH₃)2CH₂N(CH₃)2BH₃; With bis(trifluoromethanesulfonyl)amide; In toluene; at 160 ℃; for 14h; Sealed tube;

With tetrabutylammonium borohydride; In toluene;
DOI:10.1021/ja208093c

Reference yield:

: 21678-37-5
N,N,2-trimethylpropionamide

: 1350465-82-5
1,1,4,4-tetramethyl-3-phenyl-1,2-azaborolidine

: 1350465-79-0
4-benzyl-1,1,4-trimethyl-1,2-azaborolidine

: 1350465-80-3
C₆H₄(CH₂)3BHN(CH₃)2CCH₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 2 h / -30 - 0 °C

1.2: -50 - 20 °C

2.1: dimethylsulfide borane complex / tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

3.1: bis(trifluoromethanesulfonyl)amide / toluene / 14 h / 160 °C / Sealed tube

With dimethylsulfide borane complex; bis(trifluoromethanesulfonyl)amide; lithium diisopropyl amide; In tetrahydrofuran; toluene;
DOI:10.1021/ja208093c

Reference yield:

: 16487-55-1
N,N,2,2-tetramethyl-3-phenylpropanamide

: 1350465-82-5
1,1,4,4-tetramethyl-3-phenyl-1,2-azaborolidine

: 1350465-79-0
4-benzyl-1,1,4-trimethyl-1,2-azaborolidine

: 1350465-80-3
C₆H₄(CH₂)3BHN(CH₃)2CCH₃

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

2: bis(trifluoromethanesulfonyl)amide / toluene / 14 h / 160 °C / Sealed tube

With dimethylsulfide borane complex; bis(trifluoromethanesulfonyl)amide; In tetrahydrofuran; toluene;
DOI:10.1021/ja208093c