(η-Cp)Fe{PMe2Ph}(CO)(Me)

Base Information

Chemical Name:(η-Cp)Fe{PMe2Ph}(CO)(Me)
CAS No.:117228-57-6
Molecular Formula:C₁₅H₁₉FeOP
Molecular Weight:302.136
Hs Code.:

Synonyms:

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Chemical Property of (η-Cp)Fe{PMe2Ph}(CO)(Me)

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Technology Process of (η-Cp)Fe{PMe2Ph}(CO)(Me)

There total 1 articles about (η-Cp)Fe{PMe2Ph}(CO)(Me) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117228-63-4
(η-Cp)Fe{PMePh2}(CO)(Me)

: 672-66-2
Dimethyl(phenyl)phosphine

: 117228-57-6
(η-Cp)Fe{PMe2Ph}(CO)(Me)

Guidance literature:: In benzene-d6; iron compd. and Ph3CH are loaded in the glovebox into an NMR tube, while liq. PPhMe2 is dissolved in a small amt. of C6D6 and transferred and rinsed into the tube, C6D6 is added, vac. line, heated to 65°C for 3-10 d; quenched by immersing in an ice bath, NMR spect.; Kinetics;

Reference yield:

: 117228-57-6
(η-Cp)Fe{PMe2Ph}(CO)(Me)

: 32993-87-6
(η-Cp)Fe(CO){P(Me)2Ph}COMe

Guidance literature:: With carbon monoxide; In acetonitrile; Electrochem. Process; carbonylation reaction in CH3CN (0.1 M tetrabutylammonium hexafluorophosphate) under 1 atm CO at 0°C using voltammetry (acetyl-ferrocene/ferrocenium couple); Kinetics;

Reference yield:

: 117228-57-6
(η-Cp)Fe{PMe2Ph}(CO)(Me)

: Fe(C₅H₅)(COCH₃)(CH₃CN)(P(C₆H₅)(CH₃)2)

Guidance literature:: With acetonitrile; In dichloromethane; Electrochem. Process; under Ar, measuring of forward and backward rate constant in CH2Cl2 soln. contg. complex and CH3CN at 0°C in the presence of 0.1 M TBAH (fast-scan cyclic voltammetry, acetyl-ferrocene/ferrocenium couple); not isolated; Kinetics;