(η-allyl)(η-cyclopentadienyl)triethylphosphinecobalt tetraphenylborate

Base Information

• Chemical Name: (η-allyl)(η-cyclopentadienyl)triethylphosphinecobalt tetraphenylborate
• CAS No.: 84365-75-3
• Molecular Formula: C₁₄H₂₅CoP*C₂₄H₂₀B
• Molecular Weight: 602.553
• Mol file: 84365-75-3.mol

Synonyms:

Chemical Property of (η-allyl)(η-cyclopentadienyl)triethylphosphinecobalt tetraphenylborate

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (η-allyl)(η-cyclopentadienyl)triethylphosphinecobalt tetraphenylborate

There total 1 articles about (η-allyl)(η-cyclopentadienyl)triethylphosphinecobalt tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

C5H5Co(C3H5)I + ammonium tetraphenylborate (14637-34-4) + triethylphosphine (554-70-1) → (η-allyl)(η-cyclopentadienyl)triethylphosphinecobalt tetraphenylborate (84365-75-3)

Guidance literature:

In acetone; Et3P adding to a soln. of Co complex in acetone, stirring for 30 min atroom temp., NH4BPh4 adding, yellow orange ppt. filtering off, washing with toluene and petroleum ether, extg. with acetone and evapg.; identified by elem. anal., IR and NMR spectra;

DOI:10.1016/S0022-328X(00)86754-6

upstream raw materials:

ammonium tetraphenylborate

triethylphosphine

Refernces