C₂₉H₃₂O₁₃

Base Information

Chemical Name:C₂₉H₃₂O₁₃
CAS No.:1361049-69-5
Molecular Formula:C₂₉H₃₂O₁₃
Molecular Weight:588.565
Hs Code.:

C<sub>29</sub>H<sub>32</sub>O<sub>13</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₂O₁₃

Chemical Property:

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Technology Process of C₂₉H₃₂O₁₃

There total 19 articles about C₂₉H₃₂O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1361049-59-3
(+)-lactiflorin

: 108-24-7
acetic anhydride

: 1361049-69-5
C₂₉H₃₂O₁₃

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-60-6
methyl (3R,5R)-5-(tert-butyldimethylsilyloxy)-3-hydroxy-6-heptenoate

: 1361049-69-5
C₂₉H₃₂O₁₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 19 h / -78 - 20 °C

1.3: 21 h / -78 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

2.2: 21 h / 20 °C

3.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

4.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

4.2: 0.5 h / 0 °C

5.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

6.1: acetone; acetonitrile / 2 h / Irradiation

6.2: 16 h / 20 °C / 760.05 Torr

7.1: t-butyldimethylsiyl triflate / hexane; dichloromethane / 12 h / 0 °C / Molecular sieve

8.1: tetrahydrofuran; diethyl ether / -78 °C

9.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C

10.1: dmap; triethylamine / 18 h / 20 °C

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

12.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 4 h / 20 °C

13.1: 20 wt.% Pd(OH)2 on activated carbon; hydrogen / ethanol / 4 h / 20 °C / 760.05 Torr

14.1: pyridine / 20 °C

With 4-methyl-morpholine; pyridine; dmap; barium hydroxide octahydrate; 20 wt.% Pd(OH)2 on activated carbon; t-butyldimethylsiyl triflate; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; methyl chloroformate; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-71-9
C₁₆H₂₆O₆Si

: 1361049-69-5
C₂₉H₃₂O₁₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

1.2: 21 h / 20 °C

2.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

3.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

3.2: 0.5 h / 0 °C

4.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

5.1: acetone; acetonitrile / 2 h / Irradiation

5.2: 16 h / 20 °C / 760.05 Torr

6.1: t-butyldimethylsiyl triflate / hexane; dichloromethane / 12 h / 0 °C / Molecular sieve

7.1: tetrahydrofuran; diethyl ether / -78 °C

8.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C

9.1: dmap; triethylamine / 18 h / 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

11.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 4 h / 20 °C

12.1: 20 wt.% Pd(OH)2 on activated carbon; hydrogen / ethanol / 4 h / 20 °C / 760.05 Torr

13.1: pyridine / 20 °C

With 4-methyl-morpholine; pyridine; dmap; barium hydroxide octahydrate; 20 wt.% Pd(OH)2 on activated carbon; t-butyldimethylsiyl triflate; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; methyl chloroformate; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/anie.201106889