Au(bis(diphenylphosphino)methane)(3,3''-diethynyl-2,2':5',2''-terthiophene^(2-))*acetone

Base Information

• Chemical Name: Au(bis(diphenylphosphino)methane)(3,3''-diethynyl-2,2':5',2''-terthiophene^(2-))*acetone
• CAS No.: 1246464-33-4
• Molecular Formula: C₃H₆O*C₄₁H₂₈Au₂P₂S₃
• Molecular Weight: 1130.83
• Mol file: 1246464-33-4.mol

Synonyms:

Chemical Property of Au(bis(diphenylphosphino)methane)(3,3''-diethynyl-2,2':5',2''-terthiophene^(2-))*acetone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Au(bis(diphenylphosphino)methane)(3,3''-diethynyl-2,2':5',2''-terthiophene^(2-))*acetone

There total 1 articles about Au(bis(diphenylphosphino)methane)(3,3''-diethynyl-2,2':5',2''-terthiophene^(2-))*acetone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

(AuPPh3)2(3,3''-diethynyl-2,2':5',2''-terthiophene(2-))*CHCl3 + acetone (67-64-1) + bis-diphenylphosphinomethane (2071-20-7) → Au(bis(diphenylphosphino)methane)(3,3''-diethynyl-2,2':5',2''-terthiophene(2-))*acetone (1246464-33-4)

Guidance literature:

In hexane; dichloromethane; Sonication; soln. Au complex and dppm in CH2Cl2 was sonicated at room temp. for 30 min, hexane was added, react. mixt. was sonicted for 9 min; ppt. was washed with hexane, dissolved in CHCl3-CH2Cl2-acetone (1:0.25:1) and left overnight, ppt. was washed with acetone; elem. anal.;

DOI:10.1021/ic100961w

upstream raw materials:

acetone

bis-diphenylphosphinomethane