methyl onate

Base Information

• Chemical Name: methyl onate
• CAS No.: 120818-46-4
• Molecular Formula: C₃₆H₃₈O₇
• Molecular Weight: 582.694

Synonyms:

Chemical Property of methyl onate

Chemical Property:

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Technology Process of methyl onate

There total 8 articles about methyl onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

p-cresol (106-44-5) + mercury(II) diacetate (1600-27-7) + methyl onate (119005-64-0) → (4R,5S,6R)-2-Acetoxy-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-carboxylic acid methyl ester (131156-49-5,131156-50-8) + methyl onate (120818-46-4)

Guidance literature:

With molecular sieve; In dichloromethane; for 4h; Ambient temperature;

Reference yield: 47.0%

methyl onate (119005-64-0) → methyl (4R,5S,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-5,6-dihydro-4H-pyran-2-carboxylate (110390-66-4) + methyl onate (120818-46-4)

Guidance literature:

With p-cresol; molecular sieve; mercury dichloride; In dichloromethane; for 6h; Heating;

Reference yield: 18.0%

p-cresol (106-44-5) + methyl onate (119005-64-0) → methyl (4R,5S,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-5,6-dihydro-4H-pyran-2-carboxylate (110390-66-4) + methyl onate (120818-46-4)

Guidance literature:

With molecular sieve; mercury dichloride; In dichloromethane; for 6h; Heating;

upstream raw materials:

p-cresol

mercury(II) diacetate

methyl onate

methyl onate

Downstream raw materials:

(4R,5S,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-p-tolyloxy-tetrahydro-pyran-2-carboxylic acid

p-tolyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-gluco-pyranoside

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