Technology Process of C20H25N3O4
There total 6 articles about C20H25N3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 120 ℃;
Inert atmosphere;
Microwave irradiation;
DOI:10.1021/jm301059b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrazine hydrate / ethanol; water / 18 h / 50 °C
2: sodium hydride / N,N-dimethyl-formamide; acetonitrile; mineral oil / 0.33 h / 120 °C / Inert atmosphere
3: ammonium formate; palladium 10% on activated carbon / dichloromethane; methanol / 40 °C
4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 120 °C / Inert atmosphere; Microwave irradiation
With
palladium 10% on activated carbon; ammonium formate; sodium hydride; hydrazine hydrate;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1021/jm301059b
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium diisopropyl amide / tetrahydrofuran; hexane; diethyl ether / -40 - 20 °C
2: hydrazine hydrate / ethanol; water / 18 h / 50 °C
3: sodium hydride / N,N-dimethyl-formamide; acetonitrile; mineral oil / 0.33 h / 120 °C / Inert atmosphere
4: ammonium formate; palladium 10% on activated carbon / dichloromethane; methanol / 40 °C
5: sodium hydride / N,N-dimethyl-formamide; mineral oil / 120 °C / Inert atmosphere; Microwave irradiation
With
palladium 10% on activated carbon; ammonium formate; sodium hydride; hydrazine hydrate; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1021/jm301059b