{ReO(P(C₆H₅)2C₆H₄NH)2OC₂H₅}

Base Information

Chemical Name:{ReO(P(C₆H₅)2C₆H₄NH)2OC₂H₅}
CAS No.:147392-58-3
Molecular Formula:C₃₈H₃₅N₂O₂P₂Re
Molecular Weight:799.863
Hs Code.:

{ReO(P(C<sub>6</sub>H<sub>5</sub>)2C<sub>6</sub>H<sub>4</sub>NH)2OC<sub>2</sub>H<sub>5</sub>}

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Chemical Property of {ReO(P(C₆H₅)2C₆H₄NH)2OC₂H₅}

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Technology Process of {ReO(P(C₆H₅)2C₆H₄NH)2OC₂H₅}

There total 3 articles about {ReO(P(C₆H₅)2C₆H₄NH)2OC₂H₅} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: tetra-n-butylammonium tetrachlorooxorhenate(V)

: 64-17-5
ethanol

: 65423-44-1
(2-diphenylphosphino)benzeneamine

: 147392-58-3
{ReO(P(C₆H₅)2C₆H₄NH)2OC₂H₅}

Guidance literature:: With NEt₃; ethylene glycol; In ethanol; addition of 0.5 ml of ethylene glycol and 2.0 mmol of NEt3 to a solution of 0.19 mmol of (NBu4)(ReOCl4) in 4 ml EtOH, addition of 0.38 mmol of the phosphine and stirring at 25°C for 1 hour;; washing with EtOH and drying under vacuum; elem. anal., UV-, IR-, NMR spectroscopy, X-ray diffraction;;
DOI:10.1039/DT9930000605

Reference yield:

: Re(C₆H₄(P(C₆H₅)2)(NH))2(C₆H₄(P(C₆H₅)2)(NH₂))⁽¹⁺⁾*Cl^(1-)={Re(C₆H₄(P(C₆H₅)2)(NH))2(C₆H₄(P(C₆H₅)2)(NH₂))}Cl

: 147392-58-3
{ReO(P(C₆H₅)2C₆H₄NH)2OC₂H₅}

Guidance literature:: With ethanol; triethylamine; In dichloromethane; NEt3 is added to a soln. of the starting complex in CH2Cl2, then EtOH is slowly diffused into the soln.;
DOI:10.1107/S0108270193010029