1,1'-bis(2-phenyl-ortho-carboranyl)trisulfide

Base Information

Chemical Name:1,1'-bis(2-phenyl-ortho-carboranyl)trisulfide
CAS No.:778595-93-0
Molecular Formula:C₁₆H₃₀B₂₀S₃
Molecular Weight:534.832
Hs Code.:

Synonyms:

Suppliers and Price of 1,1'-bis(2-phenyl-ortho-carboranyl)trisulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,1'-bis(2-phenyl-ortho-carboranyl)trisulfide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,1'-bis(2-phenyl-ortho-carboranyl)trisulfide

There total 1 articles about 1,1'-bis(2-phenyl-ortho-carboranyl)trisulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 16390-61-7
1-phenyl-1,2-closo-C₂B₁₀H₁₁

: 7704-34-9
sulfur

: 778595-93-0
1,1'-bis(2-phenyl-ortho-carboranyl)trisulfide

: 17522-85-9
1-mercapto-2-phenyl-ortho-carborane

Guidance literature:: With sodium hydride; In 1,2-dimethoxyethane; under N2 atm. 1-phenyl-ortho-carborane and powder sulfur were added to stirred soln. NaH in 60% paraffin in DME and refluxed for 10 h; react. mixt. was cooled, diluted with MeOH, solvent was removed in vacuo, residue was diluted with water and extd. with benzene, benzene extractwas dried over MgSO4, solvent was removed in vacuo, residue was recryst d. from 40-60 pet.ether; elem. anal.;
DOI:10.1039/b406422d