Cr(CO)3C₆H₅CH₂CH₂C(C₆H₅)NC₆H₅

Base Information

Chemical Name:Cr(CO)3C₆H₅CH₂CH₂C(C₆H₅)NC₆H₅
CAS No.:84415-04-3
Molecular Formula:C₂₄H₁₉CrNO₃
Molecular Weight:421.416
Hs Code.:

Cr(CO)3C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>CH<sub>2</sub>C(C<sub>6</sub>H<sub>5</sub>)NC<sub>6</sub>H<sub>5</sub>

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Chemical Property of Cr(CO)3C₆H₅CH₂CH₂C(C₆H₅)NC₆H₅

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Technology Process of Cr(CO)3C₆H₅CH₂CH₂C(C₆H₅)NC₆H₅

There total 1 articles about Cr(CO)3C₆H₅CH₂CH₂C(C₆H₅)NC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 12170-15-9
[(1,2,3,4,5,6-η)benzaldehyde]tricarbonylchromium

: 62-53-3
aniline

: 20913-05-7,859-65-4
(Benzoylmethylene)triphenylphosphorane

: 84415-04-3,75908-47-3
Cr(CO)3C₆H₅CH₂CH₂C(C₆H₅)NC₆H₅

Guidance literature:: With H₂; Pd#C; TiCl₄; In ethanol; toluene; benzene; byproducts: TiO2; Cr complex and ylide refluxing in anhyd. C6H6 for 22 h, evapg., chromg.on SiO2, reducing with H2 on Pd/C in EtOH for 22 h, evapg., PhNH2 in anhyd. toluene adding, stirring at ambient temp., TiCl4 in toluene adding,refluxing for 3 h, TiO2 filtering off; purified by recrystn. from ether/hexane; identified by elem. anal., IR and NMR spectra;
DOI:10.1016/S0022-328X(00)86752-2

Reference yield: 100.0%

: 84415-04-3,75908-47-3
Cr(CO)3C₆H₅CH₂CH₂C(C₆H₅)NC₆H₅

: 75908-43-9
Cr(CO)2C₆H₅CH₂CH₂C(C₆H₅)NC₆H₅

Guidance literature:: In benzene; Irradiation (UV/VIS); imine complex irradiating with a high pressure Hg lamp for 1 h in anhyd. benzene under N2 with IR monitoring; color changing from right yellow to dark red; reaction is complete in 1-2 h; purified by recrystn. from ether/hexane at -30°C; identified by elem. anal., IR, NMR spectra and single crystal X-ray diffraction;
DOI:10.1016/S0022-328X(00)86752-2