RhCOCl(C₆H₅)2PC₆H₄COOCH₃

Base Information

Chemical Name:RhCOCl(C₆H₅)2PC₆H₄COOCH₃
CAS No.:625385-15-1
Molecular Formula:C₂₁H₁₇ClO₃PRh
Molecular Weight:486.696
Hs Code.:

RhCOCl(C<sub>6</sub>H<sub>5</sub>)2PC<sub>6</sub>H<sub>4</sub>COOCH<sub>3</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of RhCOCl(C₆H₅)2PC₆H₄COOCH₃

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Technology Process of RhCOCl(C₆H₅)2PC₆H₄COOCH₃

There total 1 articles about RhCOCl(C₆H₅)2PC₆H₄COOCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.5%

: di(rhodium)tetracarbonyl dichloride

: 79932-99-3
methyl 2-diphenylphosphinobenzoate

: 625385-15-1
RhCOCl(C₆H₅)2PC₆H₄COOCH₃

Guidance literature:: In dichloromethane; a soln. of phosphine-compound in CH2Cl2 was added dropwise to a soln. ofcomplex in CH2Cl2 with stirring under N2, the mixt. was stirred at room temp. for about 1 h; evapd., washed with diethyl ether, stored over silica gel in a desiccator; elem. anal.;
DOI:10.1039/b301674a

Reference yield:

: 625385-15-1
RhCOCl(C₆H₅)2PC₆H₄COOCH₃

: 74-88-4
methyl iodide

: 625385-18-4
RhCOCH₃ClI(C₆H₅)2PC₆H₄COOCH₃

Guidance literature:: In dichloromethane; the mixt. in CH2Cl2 was stirred at room temp. under N2 for about 6 h; evapd., washed with diethyl ether, stored over silica gel in a desiccator; elem. anal; Kinetics;
DOI:10.1039/b301674a