trans-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H]

Base Information

Chemical Name:trans-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H]
CAS No.:878659-76-8
Molecular Formula:C₄₃H₃₇NO₂P₂Ru
Molecular Weight:762.79
Hs Code.:

trans-N,H-[Ru(PPh<sub>3</sub>)2(CO)(NC<sub>4</sub>H<sub>3</sub>C(O)CH<sub>3</sub>)H]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H]

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Technology Process of trans-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H]

There total 6 articles about trans-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 878659-77-9
[Ru(PPh₃)3(NC₄H₃C(O)CH₃)H]

: 201230-82-2
carbon monoxide

: 878659-76-8,878659-80-4,879016-28-1
cis-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H]

: 878659-76-8,878659-80-4,879016-28-1
trans-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H]

Guidance literature:: In benzene; using Schlenk technique; a benzene suspn. of Ru-contg. compd. (0.60 mmol) was stirred under 1 atm of CO for 30 min (the color changed from from pale yellow to colourless); the soln. was concd. and hexane was added; the ppt. was filtered, washedwith hexane and dried in vac.; elem. anal.;
DOI:10.1016/j.ica.2005.05.021

Reference yield: 87.0%

: 878659-77-9
[Ru(PPh₃)3(NC₄H₃C(O)CH₃)H]

: 201230-82-2
carbon monoxide

: 878659-76-8,878659-80-4,879016-28-1
cis-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H]

: 878659-76-8,878659-80-4,879016-28-1
trans-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H]

Guidance literature:: In benzene; using Schlenk technique; a benzene suspn. of Ru-contg. compd. (0.60 mmol) was stirred under 1 atm of CO for 30 min (the color changed from from pale yellow to colourless); the soln. was concd. and hexane was added; the ppt. was filtered, washedwith hexane and dried in vac.; elem. anal.;
DOI:10.1016/j.ica.2005.05.021

Reference yield: 43.0%

: 22337-78-6
carbonyldihydridotris(triphenylphosphine)ruthenium(II)

: 358640-82-1
2-acetyl-1-(diphenylphosphanyl)pyrrole

: 878659-76-8,878659-80-4,879016-28-1
cis-N,H-[Ru(PPh₃)2(CO)(NC₄H₃C(O)CH₃)H]

Guidance literature:: In toluene; using Schlenk technique; a soln. of Ru-contg. compd. (0.51 mmol) and PPh2-contg. compd. (0.66 mmol) in toluene was refluxed for 2 h; the solvent was removed; methanol was added and the mixt. was stirred for 3 h; the solid was isolated by filter cannula, washed with methanol and hexane and dried under vac.; elem. anal.;
DOI:10.1016/j.ica.2005.05.021