(R)-2-(diphenylthiophosphinoferrocenyl)(acetoxy)methane

Base Information

Chemical Name:(R)-2-(diphenylthiophosphinoferrocenyl)(acetoxy)methane
CAS No.:896465-43-3
Molecular Formula:C₂₅H₂₃FeO₂PS
Molecular Weight:474.343
Hs Code.:

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Chemical Property of (R)-2-(diphenylthiophosphinoferrocenyl)(acetoxy)methane

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Technology Process of (R)-2-(diphenylthiophosphinoferrocenyl)(acetoxy)methane

There total 2 articles about (R)-2-(diphenylthiophosphinoferrocenyl)(acetoxy)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 896126-21-9,896465-42-2
(R)-2-(diphenylthiophosphinoferrocenylmethyl) ephedrine

: 108-24-7
acetic anhydride

: 896465-43-3,74286-49-0
(R)-2-(diphenylthiophosphinoferrocenyl)(acetoxy)methane

Guidance literature:: In acetic anhydride; Fe complex was dissolved in anhydride in Schlenk tube under Ar; soln. was stirred at 120°C for 16 h; cooled to room temp.; solvent removed (vac.); chromd. (silica gel, pentane/ether, 1/1); elem. anal.;
DOI:10.1016/j.jorganchem.2005.11.053

Reference yield: 84.0%

: 74311-50-5,74311-52-7,74286-04-7
(R)-[2-(N,N-dimethylaminomethyl)ferrocenyl]diphenylphosphine sulfide

: 896465-43-3,74286-49-0
(S)-1-diphenylthiophosphinyl-2-(acetoxymethyl)ferrocene

Guidance literature:: With acetic anhydride; heated at 100°C for 20 h in a sealed glass tube; addition of benzene, washing with aq. NaOH and water, drying over Na2SO4, evapn., column chromy. (alumina, ethyl acetate); elem. anal.;
DOI:10.1246/bcsj.53.1138