(R)-1-diphenylthiophosphinyl-2-(dimethylaminomethyl)ferrocene

Base Information

Chemical Name:(R)-1-diphenylthiophosphinyl-2-(dimethylaminomethyl)ferrocene
CAS No.:74311-50-5
Molecular Formula:C₂₅H₂₆FeNPS
Molecular Weight:459.375
Hs Code.:

Synonyms:

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Chemical Property of (R)-1-diphenylthiophosphinyl-2-(dimethylaminomethyl)ferrocene

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Technology Process of (R)-1-diphenylthiophosphinyl-2-(dimethylaminomethyl)ferrocene

There total 4 articles about (R)-1-diphenylthiophosphinyl-2-(dimethylaminomethyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 10544-50-0
sulfur

: rac-2-(N,N-dimethylaminomethyl)-1-diphenylphosphanylferrocene

: 74311-52-7,74311-50-5,74286-04-7
[2-(N,N-dimethylaminomethyl)ferrocenyl]diphenylphosphine sulfide

Guidance literature:: In dichloromethane; S8 was added to soln. of Fe complex in CH2Cl2 in Schlenk technique underAr; soln. was refluxed for 2 h; chromd. (silica gel, pentane, ether);
DOI:10.1016/j.jorganchem.2005.11.053

Reference yield: 89.0%

: rac-2-(N,N-dimethylaminomethyl)-1-diphenylphosphanylferrocene

: 7704-34-9
sulfur

: 74311-52-7,74311-50-5,74286-04-7
[2-(N,N-dimethylaminomethyl)ferrocenyl]diphenylphosphine sulfide

Guidance literature:: In benzene; refluxed for 1 h; evapn. in vac., chromy. (alumina);
DOI:10.1246/bcsj.53.1138

Reference yield: 57.0%

: 74311-52-7,74311-50-5,74286-04-7
[2-(N,N-dimethylaminomethyl)ferrocenyl]diphenylphosphine sulfide

: 74311-50-5,74311-52-7,74286-04-7
(R)-[2-(N,N-dimethylaminomethyl)ferrocenyl]diphenylphosphine sulfide

: 74311-52-7,74286-04-7,74311-50-5
(R)-1-diphenylthiophosphinyl-2-(dimethylaminomethyl)ferrocene

Guidance literature:: With O,O'-dibenzoyl-D-tartaric acid; In benzene; addition of hot benzene soln. of acid to a hot soln. of complex; evapn. in vac., dissolving in hot ethanol, addition of aq. Na2CO3, addition of dibenzoyl-d-tartaric acid in CH2Cl2 and ethanol, slow evapn. at 50°C, treatment with aq. Na2CO3, column chromy. (alumina, ether);elem. anal.;
DOI:10.1246/bcsj.53.1138