C₂₃H₂₁F₇O₂

Base Information

Chemical Name:C₂₃H₂₁F₇O₂
CAS No.:1007593-95-4
Molecular Formula:C₂₃H₂₁F₇O₂
Molecular Weight:462.407
Hs Code.:

C<sub>23</sub>H<sub>21</sub>F<sub>7</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₁F₇O₂

Chemical Property:

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Technology Process of C₂₃H₂₁F₇O₂

There total 8 articles about C₂₃H₂₁F₇O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1007592-12-2
C₁₇H₁₆F₆O₂

: 352-13-6
4-flourophenylmagnesium bromide

: 1007591-49-2
C₂₃H₂₁F₇O₂

: 1007593-95-4
C₂₃H₂₁F₇O₂

Guidance literature:: 4-flourophenylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 0.5h; Inert atmosphere;

C₁₇H₁₆F₆O₂; With chloro-trimethyl-silane; In tetrahydrofuran; diethyl ether; at -70 - 0 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol1030348

Reference yield:

: 1007591-88-9
(S)-3-hydroxycyclopent-1-enecarbonitrile

: 1007591-49-2
C₂₃H₂₁F₇O₂

: 1007593-95-4
C₂₃H₂₁F₇O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: diethylzinc / tetrahydrofuran; hexane / 0.5 h / Cooling with ice; Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: diethyl ether; tert-butyl methyl ether / 1 h / 0 °C / Inert atmosphere

3.2: -70 - -40 °C / Inert atmosphere

3.3: -40 - 20 °C / Inert atmosphere

4.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C / Inert atmosphere

4.2: -70 - 0 °C / Inert atmosphere

With dmap; copper(l) iodide; diethylzinc; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; tert-butyl methyl ether;
DOI:10.1021/ol1030348

Reference yield:

: 1007591-93-6
C₁₇H₁₃NO₂

: 1007591-49-2
C₂₃H₂₁F₇O₂

: 1007593-95-4
C₂₃H₂₁F₇O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethylzinc / tetrahydrofuran; hexane / 0.5 h / Cooling with ice; Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: diethyl ether; tert-butyl methyl ether / 1 h / 0 °C / Inert atmosphere

2.2: -70 - -40 °C / Inert atmosphere

2.3: -40 - 20 °C / Inert atmosphere

3.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C / Inert atmosphere

3.2: -70 - 0 °C / Inert atmosphere

With copper(l) iodide; diethylzinc; In tetrahydrofuran; diethyl ether; hexane; tert-butyl methyl ether;
DOI:10.1021/ol1030348